(4-METHOXYPHENYL)(3-METHYL-1-BENZOFURAN-2-YL)METHANONE

Base Information

• Chemical Name: (4-METHOXYPHENYL)(3-METHYL-1-BENZOFURAN-2-YL)METHANONE
• CAS No.: 32730-15-7
• Molecular Formula: C17H14O3
• Molecular Weight: 266.296
• Mol file: 32730-15-7.mol

Synonyms:(4-Methoxy-phenyl)-(3-methyl-benzofuran-2-yl)-methanone;2-(p-Methoxybenzoyl)-3-methyl-benzofuran;

Chemical Property of (4-METHOXYPHENYL)(3-METHYL-1-BENZOFURAN-2-YL)METHANONE

Chemical Property:

• Melting Point: 231 - 233 °C
• Boiling Point: 401.2±35.0 °C(Predicted)
• PSA: 39.44000
• Density: 1.184±0.06 g/cm3(Predicted)
• LogP: 3.98080

Purity/Quality:

99% ^*data from raw suppliers

(4-METHOXYPHENYL)(3-METHYL-1-BENZOFURAN-2-YL)METHANONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4-METHOXYPHENYL)(3-METHYL-1-BENZOFURAN-2-YL)METHANONE

There total 5 articles about (4-METHOXYPHENYL)(3-METHYL-1-BENZOFURAN-2-YL)METHANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-methoxyphenylboronic acid (5720-07-0) + 2-(2-acetylphenoxy)acetonitrile (58430-35-6) → (4-methoxyphenyl)-(3-methylbenzofuran-2-yl)methanone (32730-15-7)

Guidance literature:

With 6,6'-dimethyl-2,2'-bipyridine; palladium(II) trifluoroacetate; trifluoroacetic acid; In 2-methyltetrahydrofuran; at 80 ℃; for 24h; chemoselective reaction; Schlenk technique;

DOI:10.1039/c9ob02408e

Reference yield: 94.0%

C20H22O3Si (1422044-73-2) → (4-methoxyphenyl)-(3-methylbenzofuran-2-yl)methanone (32730-15-7)

Guidance literature:

With potassium phosphate; 1-butyl-3-methylimidazolium Tetrafluoroborate; for 0.5h; Sonication; Green chemistry;

DOI:10.1039/c2ra22355d

Reference yield: 82.0%

p-methoxybenzoylmethanol (4136-21-4) + o-hydroxyacetophenone (118-93-4,104809-67-8) → (4-methoxyphenyl)-(3-methylbenzofuran-2-yl)methanone (32730-15-7)

Guidance literature:

o-hydroxyacetophenone; With bismuth(lll) trifluoromethanesulfonate; In nitromethane; at 25 ℃; for 0.166667h; Green chemistry;

p-methoxybenzoylmethanol; In nitromethane; at 60 ℃; for 12h; chemoselective reaction; Green chemistry;

DOI:10.1002/adsc.202100143

upstream raw materials:

C₂₀H₂₂O₃Si

N-(phenoxy)acetamide

1-(4-methoxyphenyl)-2-butyn-1-ol

4-methoxyphenylboronic acid

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