Technology Process of 3,5-Heptadienoic acid, methyl ester, (Z,E)-
There total 1 articles about 3,5-Heptadienoic acid, methyl ester, (Z,E)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iron(III)-acetylacetonate; triethylaluminum; triphenylantimony;
In
benzene;
at 80 ℃;
for 2h;
Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
high pressure;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 81 percent / LiAlH4 / diethyl ether / 3 h / 20 °C
2: 70 percent / PBr3, pyridine / hexane / 1) 0 deg C, 2 h; 2) 20 deg C, 12 h
3: 1) Li2CuCl4; 2) p-toluenesulfonic acid / 1) THF, 0 deg C, 3 h, then 20 deg C, 12 h; 2) methanol, water, 60 deg C, 3 h
4: 30 percent / C6H5SH / 2 h / 100 °C
With
pyridine; lithium aluminium tetrahydride; dilithium tetrachlorocuprate; phosphorus tribromide; toluene-4-sulfonic acid; thiophenol;
In
diethyl ether; hexane;
