Benzaldehyde, 4-[(1E)-2-[2,5-bis[(2S)-2-methylbutoxy]-4-[(1E)-2-[3,4,5-tris(dodecyloxy) phenyl]ethenyl]phenyl]ethenyl]-2,5-bis[(2S)-2-methylbutoxy]-

Base Information

Chemical Name:Benzaldehyde, 4-[(1E)-2-[2,5-bis[(2S)-2-methylbutoxy]-4-[(1E)-2-[3,4,5-tris(dodecyloxy) phenyl]ethenyl]phenyl]ethenyl]-2,5-bis[(2S)-2-methylbutoxy]-
CAS No.:328249-45-2
Molecular Formula:C79H130O8
Molecular Weight:1207.9
Hs Code.:

Benzaldehyde,
4-[(1E)-2-[2,5-bis[(2S)-2-methylbutoxy]-4-[(1E)-2-[3,4,5-tris(dodecyloxy)
phenyl]ethenyl]phenyl]ethenyl]-2,5-bis[(2S)-2-methylbutoxy]-

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Chemical Property of Benzaldehyde, 4-[(1E)-2-[2,5-bis[(2S)-2-methylbutoxy]-4-[(1E)-2-[3,4,5-tris(dodecyloxy) phenyl]ethenyl]phenyl]ethenyl]-2,5-bis[(2S)-2-methylbutoxy]-

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Technology Process of Benzaldehyde, 4-[(1E)-2-[2,5-bis[(2S)-2-methylbutoxy]-4-[(1E)-2-[3,4,5-tris(dodecyloxy) phenyl]ethenyl]phenyl]ethenyl]-2,5-bis[(2S)-2-methylbutoxy]-

There total 3 articles about Benzaldehyde, 4-[(1E)-2-[2,5-bis[(2S)-2-methylbutoxy]-4-[(1E)-2-[3,4,5-tris(dodecyloxy) phenyl]ethenyl]phenyl]ethenyl]-2,5-bis[(2S)-2-methylbutoxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 117241-34-6
(E)-N-phenyl-3,4,5-tris(dodecyloxy)benzaldimine

: 328249-44-1
(E)-4-{4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzaldehyde dimethyl acetal

: 328249-45-2
(E,E)-4-{4-(3,4,5-tridodecyloxystyryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzaldehyde

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl-formamide; at 80 ℃; for 1h;
DOI:10.1021/ja0033180

Reference yield:

: 117241-32-4
3,4,5-tris(dodecyloxy)benzaldehyde

: 328249-45-2
(E,E)-4-{4-(3,4,5-tridodecyloxystyryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 60 °C

2: 90 percent / t-BuOK / dimethylformamide / 1 h / 80 °C

With potassium tert-butylate; In N,N-dimethyl-formamide;
DOI:10.1021/ja0033180

Reference yield:

: (E)-4-{4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzaldehyde

: 328249-45-2
(E,E)-4-{4-(3,4,5-tridodecyloxystyryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / methanol / 2 h / 70 °C

2: 90 percent / t-BuOK / dimethylformamide / 1 h / 80 °C

With potassium tert-butylate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja0033180