4-{(E)-2-[4-((E)-2-{2,5-Bis-((S)-2-methyl-butoxy)-4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-2,5-bis-((S)-2-methyl-butoxy)-phenyl]-vinyl}-benzoyl chloride

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Chemical Name:4-{(E)-2-[4-((E)-2-{2,5-Bis-((S)-2-methyl-butoxy)-4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-2,5-bis-((S)-2-methyl-butoxy)-phenyl]-vinyl}-benzoyl chloride
CAS No.:889214-89-5
Molecular Formula:C₈₇H₁₃₅ClO₈
Molecular Weight:1344.48
Hs Code.:

Synonyms:4-{(E)-2-[4-((E)-2-{2,5-Bis-((S)-2-methyl-butoxy)-4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-2,5-bis-((S)-2-methyl-butoxy)-phenyl]-vinyl}-benzoyl chloride

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Chemical Property of 4-{(E)-2-[4-((E)-2-{2,5-Bis-((S)-2-methyl-butoxy)-4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-2,5-bis-((S)-2-methyl-butoxy)-phenyl]-vinyl}-benzoyl chloride

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Technology Process of 4-{(E)-2-[4-((E)-2-{2,5-Bis-((S)-2-methyl-butoxy)-4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-2,5-bis-((S)-2-methyl-butoxy)-phenyl]-vinyl}-benzoyl chloride

There total 3 articles about 4-{(E)-2-[4-((E)-2-{2,5-Bis-((S)-2-methyl-butoxy)-4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-2,5-bis-((S)-2-methyl-butoxy)-phenyl]-vinyl}-benzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 4-{(E)-2-[4-((E)-2-{2,5-Bis-((S)-2-methyl-butoxy)-4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-2,5-bis-((S)-2-methyl-butoxy)-phenyl]-vinyl}-benzoic acid

: 889214-89-5
4-{(E)-2-[4-((E)-2-{2,5-Bis-((S)-2-methyl-butoxy)-4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-2,5-bis-((S)-2-methyl-butoxy)-phenyl]-vinyl}-benzoyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b005903j

Reference yield:

: 135580-51-7
(diethyl phosphoric) 4-methylbenzoic anhydride

: 889214-89-5
4-{(E)-2-[4-((E)-2-{2,5-Bis-((S)-2-methyl-butoxy)-4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-2,5-bis-((S)-2-methyl-butoxy)-phenyl]-vinyl}-benzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: t-BuOK / dimethylformamide; tetrahydrofuran

1.2: 100 percent / KOH / ethanol / 80 °C

2.1: 100 percent / (COCl)2 / CH₂Cl₂; dimethylformamide

With oxalyl dichloride; potassium tert-butylate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1.1: Wittig-Horner reaction / 1.2: Substitution / 2.1: Substitution;
DOI:10.1039/b005903j

Reference yield:

: 328249-45-2
(E,E)-4-{4-(3,4,5-tridodecyloxystyryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzaldehyde

: 889214-89-5
4-{(E)-2-[4-((E)-2-{2,5-Bis-((S)-2-methyl-butoxy)-4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-2,5-bis-((S)-2-methyl-butoxy)-phenyl]-vinyl}-benzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: t-BuOK / dimethylformamide; tetrahydrofuran

1.2: 100 percent / KOH / ethanol / 80 °C

2.1: 100 percent / (COCl)2 / CH₂Cl₂; dimethylformamide

With oxalyl dichloride; potassium tert-butylate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1.1: Wittig-Horner reaction / 1.2: Substitution / 2.1: Substitution;
DOI:10.1039/b005903j