C₅H₉Mn(CO)4

Base Information

Chemical Name:C₅H₉Mn(CO)4
CAS No.:71713-52-5
Molecular Formula:C₉H₉MnO₄
Molecular Weight:236.106
Hs Code.:

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Chemical Property of C₅H₉Mn(CO)4

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Technology Process of C₅H₉Mn(CO)4

There total 1 articles about C₅H₉Mn(CO)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 10170-69-1
dimanganese decacarbonyl

: 598-25-4
Dimethylallene

: (η3-CH2CHC(CH3)2)Mn(CO)4

: 71713-52-5
C₅H₉Mn(CO)4

: 107883-18-1
tricarbonyl-η(3:CH)-2-methyl-E-3-(3(8),6-m-menthadiene-6-yl)-2-butene-1-yl-manganese

: octacarbonyl-μ-η(2:2)-1.1-dimethylallene-dimanganese(0)

: hexacarbonyl-μ-η(3:CH:3:CH)-2,3,4,5-tetramethyl-2,5-hexadiene-1,4-diyl-dimanganese

Guidance literature:: In hexane; Irradiation (UV/VIS); IR-conducted UV irradiation of a solution of 2.13 mmol of Mn2(CO)10 and20 mmol 1.1-dimethylallene in 700 ml n-hexane at 248 K under N2, filtration and evaporation;; HPLC (n-hexane, 3rd, 5th and 6th zone (octa-, tri- or hexacarbonyl compound), recrystallization from n-hexane at 183 K); 2nd zone (tetracarbonyl compounds) (yield 12 %, purification by distillation); elem. anal., NMR and IR spectroscopy;;
DOI:10.1016/0022-328X(86)80085-7