(E)-2-(4-CHLORO-2-NITROPHENYL)-N,N-DIMETHYL-1-ETHENAMINE

Base Information

• Chemical Name: (E)-2-(4-CHLORO-2-NITROPHENYL)-N,N-DIMETHYL-1-ETHENAMINE
• CAS No.: 32989-56-3
• Molecular Formula: C10H11ClN2O2
• Molecular Weight: 226.663
• Hs Code.: 2921490090
• Mol file: 32989-56-3.mol

Synonyms:(E)-2-(4-chloro-2-nitrophenyl)-N,N-dimethylethenamine;(E)-2-(4-chloro-2-nitrophenyl)-N,N-dimethylethyleneamine;trans-4-chloro-β-dimethylamino-2-nitrostyrene;

Chemical Property of (E)-2-(4-CHLORO-2-NITROPHENYL)-N,N-DIMETHYL-1-ETHENAMINE

Chemical Property:

• PSA: 49.06000
• LogP: 3.30370

Purity/Quality:

99% ^*data from raw suppliers

(E)-2-(4-CHLORO-2-NITROPHENYL)-N,N-DIMETHYL-1-ETHENAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (E)-2-(4-CHLORO-2-NITROPHENYL)-N,N-DIMETHYL-1-ETHENAMINE

There total 4 articles about (E)-2-(4-CHLORO-2-NITROPHENYL)-N,N-DIMETHYL-1-ETHENAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-chloro-2-nitrotoluene (89-59-8) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → 5-chloro-trans-2-[β-(dimethylamino)vinyl]-nitrobenzene (32989-56-3)

Guidance literature:

With copper(l) iodide; N,N-dimethyl-formamide; at 180 ℃; for 0.166667h; under 6000.6 - 7500.75 Torr; microwave irradiation;

DOI:10.1039/b313012f

Reference yield:

4-chloro-2-nitrotoluene (89-59-8) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → 4-chloro-1-[(2-dimethylamino)ethenyl]-2-nitrobenzene (32989-56-3)

Guidance literature:

With pyrrolidine; for 24h; Heating;

DOI:10.1080/00304940609355993

Reference yield:

tert-Butoxybis(dimethylamino)methane (5815-08-7) + 4-chloro-2-nitrotoluene (89-59-8) → 4-chloro-1-[(2-dimethylamino)ethenyl]-2-nitrobenzene (32989-56-3)

Guidance literature:

upstream raw materials:

4-chloro-2-nitrotoluene

N,N-dimethyl-formamide dimethyl acetal

tert-Butoxybis(dimethylamino)methane

Downstream raw materials:

4-Chloro-2-nitrobenzaldehyde

(2E)-3-(2-amino-4-chlorophenyl)-2-(4-chlorophenyl)prop-2-enoic acid

(2E)-3-(4-chloro-2-nitrophenyl)-2-(4-chlorophenyl)prop-2-enoic acid

methyl (2E)-3-[2-(4'-chloro-2'-nitrostyryl)-1-(phenylsulfonyl)indol-3-yl]but-2-enoate

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