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5815-08-7

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5815-08-7 Usage

Chemical Properties

Clear pale yellow liquid

Uses

Different sources of media describe the Uses of 5815-08-7 differently. You can refer to the following data:
1. Reactant for:? ;Preparation of pyrroloquinazolines as photochemotherapeutic agents1? ;Enanatioslective formal synthesis of the Cinchona alkaloid quinine via stereoselective intermolecular radical addition2? ;Synthesis of camptothecin via intramolecular isomuenchnone cycloaddition reaction3? ;Aminomethylenation reactions4
2. Mild enamination reagent; catalyst in ring-opening polymerization reactions.
3. Reactant for:Preparation of pyrroloquinazolines as photochemotherapeutic agentsEnanatioslective formal synthesis of the Cinchona alkaloid quinine via stereoselective intermolecular radical additionSynthesis of camptothecin via intramolecular isomuenchnone cycloaddition reactionAminomethylenation reactions

Check Digit Verification of cas no

The CAS Registry Mumber 5815-08-7 includes 7 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 4 digits, 5,8,1 and 5 respectively; the second part has 2 digits, 0 and 8 respectively.
Calculate Digit Verification of CAS Registry Number 5815-08:
(6*5)+(5*8)+(4*1)+(3*5)+(2*0)+(1*8)=97
97 % 10 = 7
So 5815-08-7 is a valid CAS Registry Number.
InChI:InChI=1/C9H22N2O/c1-9(2,3)12-8(10(4)5)11(6)7/h8H,1-7H3/p+2

5815-08-7 Well-known Company Product Price

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  • (Code)Product description
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  • Detail
  • Alfa Aesar

  • (H27861)  tert-Butoxybis(dimethylamino)methane, tech. 90%   

  • 5815-08-7

  • 1g

  • 437.0CNY

  • Detail
  • Alfa Aesar

  • (H27861)  tert-Butoxybis(dimethylamino)methane, tech. 90%   

  • 5815-08-7

  • 5g

  • 1209.0CNY

  • Detail
  • Alfa Aesar

  • (H27861)  tert-Butoxybis(dimethylamino)methane, tech. 90%   

  • 5815-08-7

  • 25g

  • 5565.0CNY

  • Detail
  • Aldrich

  • (384216)  tert-Butoxybis(dimethylamino)methane  

  • 5815-08-7

  • 384216-1G

  • 510.12CNY

  • Detail
  • Aldrich

  • (384216)  tert-Butoxybis(dimethylamino)methane  

  • 5815-08-7

  • 384216-10G

  • 2,577.51CNY

  • Detail
  • Aldrich

  • (20425)  tert-Butoxybis(dimethylamino)methane  technical

  • 5815-08-7

  • 20425-10ML-F

  • 2,887.56CNY

  • Detail
  • Aldrich

  • (20425)  tert-Butoxybis(dimethylamino)methane  technical

  • 5815-08-7

  • 20425-50ML-F

  • 12,788.10CNY

  • Detail

5815-08-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 13, 2017

Revision Date: Aug 13, 2017

1.Identification

1.1 GHS Product identifier

Product name Tert-Butoxybis(Dimethylamino)Methane

1.2 Other means of identification

Product number -
Other names N,N,N',N'-tetramethyl-1-[(2-methylpropan-2-yl)oxy]methanediamine

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:5815-08-7 SDS

5815-08-7Synthetic route

potassium tert-butylate
865-47-4

potassium tert-butylate

N,N,N',N'-tetramethylformamidinium methyl sulfate
2013-91-4

N,N,N',N'-tetramethylformamidinium methyl sulfate

tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

Conditions
ConditionsYield
In diethyl ether for 1h;67%
Bis(dimethylamino)acetonitrile
2214-82-6

Bis(dimethylamino)acetonitrile

potassium tert-butylate
865-47-4

potassium tert-butylate

tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

Conditions
ConditionsYield
In diethyl ether
potassium tert-butylate
865-47-4

potassium tert-butylate

N,N,N',N'-tetramethylformamidinium hexafluorophosphate

N,N,N',N'-tetramethylformamidinium hexafluorophosphate

A

tris(dimethylamino)methane
5762-56-1

tris(dimethylamino)methane

B

tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

C

N,N-dimethylformamide di-tert-butyl acetal
36805-97-7

N,N-dimethylformamide di-tert-butyl acetal

Conditions
ConditionsYield
In tetrahydrofuran at 50℃; for 1h;
potassium tert-butylate
865-47-4

potassium tert-butylate

N,N,N',N'-tetramethylformamidinium methyl sulfate
2013-91-4

N,N,N',N'-tetramethylformamidinium methyl sulfate

A

tris(dimethylamino)methane
5762-56-1

tris(dimethylamino)methane

B

tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

C

N,N-dimethylformamide di-tert-butyl acetal
36805-97-7

N,N-dimethylformamide di-tert-butyl acetal

Conditions
ConditionsYield
In tetrahydrofuran at 60℃; for 1h;
potassium tert-butylate
865-47-4

potassium tert-butylate

N,N,N',N'-Tetramethylformamidinium-(p-toluolsulfonat)
3218-35-7

N,N,N',N'-Tetramethylformamidinium-(p-toluolsulfonat)

A

tris(dimethylamino)methane
5762-56-1

tris(dimethylamino)methane

B

tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

C

N,N-dimethylformamide di-tert-butyl acetal
36805-97-7

N,N-dimethylformamide di-tert-butyl acetal

Conditions
ConditionsYield
In tetrahydrofuran at 50℃; for 1h;
tris(dimethylamino)methane
5762-56-1

tris(dimethylamino)methane

N,N-dimethylformamide di-tert-butyl acetal
36805-97-7

N,N-dimethylformamide di-tert-butyl acetal

tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

Conditions
ConditionsYield
at 20℃; Product distribution / selectivity;
potassium tert-butylate
865-47-4

potassium tert-butylate

N,N,N',N'-tetramethylformamidinium hexafluorophosphate

N,N,N',N'-tetramethylformamidinium hexafluorophosphate

tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

Conditions
ConditionsYield
In tetrahydrofuran at 20 - 60℃; for 4.5h; Inert atmosphere;
tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

5-(2,4-difluorophenoxy)-6-nitroindan
81614-72-4

5-(2,4-difluorophenoxy)-6-nitroindan

[6-(2,4-Difluoro-phenoxy)-5-nitro-indan-(1E)-ylidenemethyl]-dimethyl-amine
82505-46-2

[6-(2,4-Difluoro-phenoxy)-5-nitro-indan-(1E)-ylidenemethyl]-dimethyl-amine

Conditions
ConditionsYield
at 155 - 160℃; for 2h;100%
tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

benzyl 3-phenoxyphenyl ketone
632365-56-1

benzyl 3-phenoxyphenyl ketone

C23H21NO2
632365-57-2

C23H21NO2

Conditions
ConditionsYield
In toluene at 20 - 60℃; for 16h;100%
tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

7-Methyl-4-nitrobenzo[b]furan
325708-09-6

7-Methyl-4-nitrobenzo[b]furan

N,N-[dimethyl] (2-(4-nitrobenzofur-7-yl)vinyl)amine
603305-64-2

N,N-[dimethyl] (2-(4-nitrobenzofur-7-yl)vinyl)amine

Conditions
ConditionsYield
for 0.666667h; Heating / reflux;100%
for 0.666667h; Heating / reflux;100%
tert-butyl 1-(4-bromothiophen-2-yl)-4-oxocyclohexylcarbamate
874199-33-4

tert-butyl 1-(4-bromothiophen-2-yl)-4-oxocyclohexylcarbamate

tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

(E)-tert-butyl 1-(4-bromothiophen-2-yl)-3-((dimethylamino)methylene)-4-oxocyclohexylcarbamate
874199-34-5

(E)-tert-butyl 1-(4-bromothiophen-2-yl)-3-((dimethylamino)methylene)-4-oxocyclohexylcarbamate

Conditions
ConditionsYield
In toluene at 20 - 80℃;100%
In toluene at 20 - 80℃;
(RS)-2-phenylcyclohexanone
1444-65-1

(RS)-2-phenylcyclohexanone

tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

2-[1-dimethylaminometh-(Z)-ylidene]-6-phenylcyclohexanone
1172638-49-1

2-[1-dimethylaminometh-(Z)-ylidene]-6-phenylcyclohexanone

Conditions
ConditionsYield
at 110℃; for 1.25h; Neat (no solvent);100%
(±)-tert-butyl 4-oxo-3-phenylpiperidine-1-carboxylate
632352-56-8

(±)-tert-butyl 4-oxo-3-phenylpiperidine-1-carboxylate

tert-Butoxybis(dimethylamino)methane
5815-08-7

tert-Butoxybis(dimethylamino)methane

3-[1-dimethylaminometh-(Z)-ylidene]-4-oxo-5-phenylpiperidine-1-carboxylic acid tert-butyl ester
1172638-56-0

3-[1-dimethylaminometh-(Z)-ylidene]-4-oxo-5-phenylpiperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
at 110℃; for 2h; Neat (no solvent);100%

5815-08-7Relevant articles and documents

NEW PROCESSES

-

Page/Page column 144, (2009/08/16)

The invention relates to a new process for producing NEP inhibitors or prodrugs thereof, in particular NEP inhibitors comprising a γ-amino-δ-biphenyl-α-methylalkanoic acid, or acid ester, backbone. In detail, the new processes, according to the present invention, are ultimately related to the synthesis of intermediates to prepare the above NEP inhibitors, namely compounds according to formula (1), or salt thereof, wherein R1 and R2 are, independently of each other, hydrogen or a nitrogen protecting group, and R3 is a carboxyl group or an ester group, preferably carboxyl group or alkyl ester.

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