5-Pyrimidinemethanol, 4-[[(3-chloro-4-methoxyphenyl)methyl]amino]-2-(methylthio)-

Base Information

• Chemical Name: 5-Pyrimidinemethanol, 4-[[(3-chloro-4-methoxyphenyl)methyl]amino]-2-(methylthio)-
• CAS No.: 330785-85-8
• Molecular Formula: C14H16ClN3O2S
• Molecular Weight: 325.819
• Hs Code.: 2933599090

Synonyms:(4-((3-Chloro-4-methoxybenzyl)amino)-2-(methylthio)pyrimidin-5-yl)methanol;

Chemical Property of 5-Pyrimidinemethanol, 4-[[(3-chloro-4-methoxyphenyl)methyl]amino]-2-(methylthio)-

Chemical Property:

• PSA: 95.80000
• LogP: 2.38680

Purity/Quality:

≥99% ^*data from raw suppliers

(4-((3-Chloro-4-methoxybenzyl)amino)-2-(methylthio)pyrimidin-5-yl)methanol 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Pyrimidinemethanol, 4-[[(3-chloro-4-methoxyphenyl)methyl]amino]-2-(methylthio)-

There total 3 articles about 5-Pyrimidinemethanol, 4-[[(3-chloro-4-methoxyphenyl)methyl]amino]-2-(methylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ [4-(3-Chloro-4-methoxy-benzylamino)-2-methylsulfanyl-pyrimidin-5-yl]-methanol (330785-85-8) + di-isopropyl ether (108-20-3)

Guidance literature:

Reference yield:

ethyl 4-[(3-chloro-4-methoxybenzyl)amino]-2-(methylsulfanyl)pyrimidine-5-carboxylate (330785-81-4) → [4-(3-Chloro-4-methoxy-benzylamino)-2-methylsulfanyl-pyrimidin-5-yl]-methanol (330785-85-8)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran;

Reference yield:

ethyl 4-[(3-chloro-4-methoxybenzyl)amino]-2-(methylsulfanyl)pyrimidine-5-carboxylate (330785-81-4) + di-isopropyl ether (108-20-3) → [4-(3-Chloro-4-methoxy-benzylamino)-2-methylsulfanyl-pyrimidin-5-yl]-methanol (330785-85-8)

Guidance literature:

With sodium hydroxide; magnesium sulfate; In tetrahydrofuran; water; ethyl acetate;

upstream raw materials:

ethyl 4-[(3-chloro-4-methoxybenzyl)amino]-2-(methylsulfanyl)pyrimidine-5-carboxylate

di-isopropyl ether

Downstream raw materials:

4-(3-Chloro-4-methoxy-benzylamino)-2-methylsulfanyl-pyrimidine-5-carbaldehyde

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