Ethanone, 1-(4-chlorophenyl)-2-(phenylthio)-

Base Information

• Chemical Name: Ethanone, 1-(4-chlorophenyl)-2-(phenylthio)-
• CAS No.: 33192-00-6
• Molecular Formula: C14H11ClOS
• Molecular Weight: 262.76

Synonyms:1-(4-chloro-phenyl)-2-phenylsulfanyl-ethanone;α-(phenylthio)-4-chloroacetophenone;α-phenylthio-p-chloroacetophenone;1-(4-chlorophenyl)-2-(phenylthio)ethanone;1-(4-Chlor-phenyl)-2-phenylmercapto-aethanon;α-(Phenylthio)-p-chloroacetophnone;

Chemical Property of Ethanone, 1-(4-chlorophenyl)-2-(phenylthio)-

Chemical Property:

• PSA: 42.37000
• LogP: 4.31500

Purity/Quality:

99% ^*data from raw suppliers

1-(4-CHLOROPHENYL)-2-(PHENYLTHIO)ETHANONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-(4-chlorophenyl)-2-(phenylthio)-

There total 8 articles about Ethanone, 1-(4-chlorophenyl)-2-(phenylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

thiophenol (108-98-5) + 4-chlorobenzoylmethyl bromide (536-38-9) → 2-(4-chlorophenyl)ethanonyl phenyl sulfide (33192-00-6)

Guidance literature:

thiophenol; In methanol; Inert atmosphere;

4-chlorobenzoylmethyl bromide; In dimethyl sulfoxide; at 20 ℃; for 0.25h; Inert atmosphere;

DOI:10.1002/ejoc.201201422

Reference yield: 65.0%

sodium thiophenolate (930-69-8) + 2-[2-(4-Chloro-phenyl)-2-oxo-ethylsulfanyl]-1-methyl-4,6-diphenyl-pyridinium; bromide (96928-08-4) → 1-methyl-4,6-diphenyl-1H-pyridine-2-thione (26479-04-9) + 2-(4-chlorophenyl)ethanonyl phenyl sulfide (33192-00-6)

Guidance literature:

In methanol; for 2h; Heating;

Reference yield:

thiophenol (108-98-5) + 4-chlorobenzoylmethyl bromide (536-38-9) → 2-(4-Chlorophenyl)-3-[4-(2-pyrrolidinoethoxy)benzoyl]benzothiophene (63676-28-8) + 2-(4-chlorophenyl)ethanonyl phenyl sulfide (33192-00-6)

Guidance literature:

With potassium hydroxide; In ethanol; water;

upstream raw materials:

sodium thiophenolate

2-[2-(4-Chloro-phenyl)-2-oxo-ethylsulfanyl]-1-methyl-4,6-diphenyl-pyridinium; bromide

4-chlorobenzaldehyde

1-((phenylthio)methyl)-1H-benzo[d][1,2,3]triazole

Downstream raw materials:

1-(4-Chloro-phenyl)-2-(4-methoxy-phenyl)-2-phenylsulfanyl-ethanone

6-(4-chlorophenyl)-4-[4-(dimethylamino)phenyl]-2-ethoxy-5-(phenylsulfanyl)nicotinonitrile

((4-chlorophenyl)ethynyl)(phenyl)sulfane

4-(5-(4-chlorophenyl)furan-3-yl)butyl pivalate

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