TRIS(DIFORMYLAMINO)METHANE

Base Information

• Chemical Name: TRIS(DIFORMYLAMINO)METHANE
• CAS No.: 332047-72-0
• Molecular Formula: C7H7N3O6
• Molecular Weight: 229.149
• Hs Code.: 2924199090
• Mol file: 332047-72-0.mol

Synonyms:

Chemical Property of TRIS(DIFORMYLAMINO)METHANE

Chemical Property:

• Melting Point: 145 °C
• PSA: 112.14000
• LogP: 0.92980
• Storage Temp.: Refrigerator (+4°C)

Purity/Quality:

97% ^*data from raw suppliers

TRIS-(DIFORMYLAMINO)METHANE 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 37/39-26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TRIS(DIFORMYLAMINO)METHANE

There total 1 articles about TRIS(DIFORMYLAMINO)METHANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

triformylamine (25891-31-0) + sodium diformamide (18197-26-7) → tris(diformylamino)methane (332047-72-0)

Guidance literature:

In acetonitrile; at 20 ℃; for 66h;

Reference yield: 84.0%

1,3-Dimethoxybenzene (151-10-0) + tris(diformylamino)methane (332047-72-0) → 2,4-Dimethoxybenzaldehyde (613-45-6)

Guidance literature:

With trifluorormethanesulfonic acid; In nitromethane; at 20 ℃; for 2.5h;

DOI:10.1515/znb-2007-0803

Reference yield: 65.0%

o-xylene (95-47-6) + tris(diformylamino)methane (332047-72-0) → 3,4-dimethylbenzaldehyde (5973-71-7)

Guidance literature:

o-xylene; tris(diformylamino)methane; With aluminium trichloride; In 1,2-dichloro-ethane; at -19 - 0 ℃;

With water; Heating;

DOI:10.1515/znb-2002-1116

upstream raw materials:

triformylamine

sodium diformamide

Downstream raw materials:

4-methyl-benzaldehyde

2,4-Dimethoxybenzaldehyde

(4-isopropylbenzaldehyde)

4-phenoxy benzaldehyde

Refernces