5-BUTYLSULFANYL-[1,3,4]THIADIAZOL-2-YLAMINE

Base Information

• Chemical Name: 5-BUTYLSULFANYL-[1,3,4]THIADIAZOL-2-YLAMINE
• CAS No.: 33313-06-3
• Molecular Formula: C6H11N3S2
• Molecular Weight: 189.305
• Hs Code.: 2934999090
• Mol file: 33313-06-3.mol

Synonyms:5-n-Butylthio-1,3,4-thiadiazolyl-2-amin;5-butylthio-1,3,4-thiadiazole-2-ylamine;

Chemical Property of 5-BUTYLSULFANYL-[1,3,4]THIADIAZOL-2-YLAMINE

Chemical Property:

• Vapor Pressure: 8.95E-05mmHg at 25°C
• Boiling Point: 339.8oC at 760 mmHg
• Flash Point: 159.3oC
• PSA: 105.34000
• Density: 1.27g/cm3
• LogP: 2.59370

Purity/Quality:

98%min ^*data from raw suppliers

5-(Butylsulfanyl)-1,3,4-thiadiazol-2-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-BUTYLSULFANYL-[1,3,4]THIADIAZOL-2-YLAMINE

There total 3 articles about 5-BUTYLSULFANYL-[1,3,4]THIADIAZOL-2-YLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1-bromo-butane (109-65-9) + 2-Amino-5-mercapto-1,3,4-thiadiazole (2349-67-9) → 2-amino-5-butylmercapto-1,3,4-thiadiazole (33313-06-3)

Guidance literature:

2-Amino-5-mercapto-1,3,4-thiadiazole; With potassium hydroxide; In ethanol; for 0.166667h;

1-bromo-butane; In ethanol; for 2h;

DOI:10.1002/cmdc.201300244

Reference yield:

n-Butyl chloride (109-69-3) + 2-Amino-5-mercapto-1,3,4-thiadiazole (2349-67-9) → 2-amino-5-butylmercapto-1,3,4-thiadiazole (33313-06-3)

Guidance literature:

With sodium hydroxide; In methanol; water; at 20 ℃; for 10h;

DOI:10.1016/j.cclet.2012.04.005

Reference yield:

→ 2-amino-5-butylmercapto-1,3,4-thiadiazole (33313-06-3)

Guidance literature:

/BRN= 118749/;

upstream raw materials:

n-Butyl chloride

2-Amino-5-mercapto-1,3,4-thiadiazole

1-bromo-butane

Downstream raw materials:

2-butylsulfanyl-[1,3,4]thiadiazolo[3,2-a]pyrimidine-5,7-dione

6-benzyl-2-butylsulfanyl-[1,3,4]thiadiazolo[3,2-a]pyrimidine-5,7-dione

(5-butylsulfanyl-[1,3,4]thiadiazol-2-yl)-dithiocarbamic acid benzyl ester

N-(5-Butylsulfanyl-[1,3,4]thiadiazol-2-yl)-succinamic acid (3S,8S,9S,10R,13R,14S,17R)-17-((1R,4R)-4-ethyl-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

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