1-Adamantylhydrazine hydrochloride

Base Information

• Chemical Name: 1-Adamantylhydrazine hydrochloride
• CAS No.: 16782-39-1
• Molecular Formula: C₁₀H₁₈N₂*ClH
• Molecular Weight: 202.727
• DSSTox Substance ID: DTXSID90498255
• NSC Number: 194592
• Mol file: 16782-39-1.mol

Synonyms:1-Adamantylhydrazine hydrochloride;16782-39-1;1-adamantylhydrazine;hydrochloride;ADAMANTAN-1-YLHYDRAZINE HYDROCHLORIDE;Hydrazine, tricyclo[3.3.1.13,7]dec-1-yl-, hydrochloride (1:1);starbld0049622;SCHEMBL7146424;DTXSID90498255;NSC194592;NSC 194592;NSC-194592;(ADAMANTAN-1-YL)HYDRAZINE HYDROCHLORIDE;(Tricyclo[3.3.1.1~3,7~]decan-1-yl)hydrazine--hydrogen chloride (1/1)

Chemical Property of 1-Adamantylhydrazine hydrochloride

Chemical Property:

• Vapor Pressure: 0.00306mmHg at 25°C
• Boiling Point: 284°Cat760mmHg
• Flash Point: 145.7°C
• Density: 1.09g/cm³
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 202.1236763
• Heavy Atom Count: 13
• Complexity: 159

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1C2CC3CC1CC(C2)(C3)NN.Cl

Technology Process of 1-Adamantylhydrazine hydrochloride

There total 1 articles about 1-Adamantylhydrazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

1-Adamantyl bromide (768-90-1) → 1-adamantylhydrazine hydrochloride (16782-39-1)

Guidance literature:

1-Adamantyl bromide; With hydrazine hydrate; at 110 - 135 ℃;

With hydrogenchloride; In diethyl ether; water; pH=2;

DOI:10.1055/s-0040-1707353

Reference yield: 72.0%

4-trifluoromethyl-phenyl acetyl chloride (329-15-7) + adamant-1-ylhydrazine dihydrochloride (16782-39-1,20342-55-6,92234-62-3) → N'-(adamantan-1-yl)-4-(trifluoromethyl)benzohydrazide

Guidance literature:

With sodium hydroxide; In diethyl ether; water; at 20 ℃; for 1.08333h;

DOI:10.1016/j.ejmech.2021.113485

Reference yield: 63.0%

malonaldehydebis(dimethylacetal) (102-52-3) + adamant-1-ylhydrazine dihydrochloride (16782-39-1,20342-55-6,92234-62-3) → 1-((3s,5s,7s)-adamantan-1-yl)-1H-pyrazole (92234-54-3)

Guidance literature:

With sodium carbonate; In ethanol; for 2h; Heating;

DOI:10.1002/jhet.5570210149

upstream raw materials:

1-Adamantyl bromide

Downstream raw materials:

1-((3s,5s,7s)-adamantan-1-yl)-1H-pyrazole

1-(1-adamantyl)-1,2,4-triazole