4-methoxy-5-[(2Z)-2-{1-[(E)-(2-methoxy-4-nitro-5-sulfophenyl)diazenyl]-2-oxo-2-(phenylamino)ethylidene}hydrazino]-2-nitrobenzenesulfonic acid

Base Information

• Chemical Name: 4-methoxy-5-[(2Z)-2-{1-[(E)-(2-methoxy-4-nitro-5-sulfophenyl)diazenyl]-2-oxo-2-(phenylamino)ethylidene}hydrazino]-2-nitrobenzenesulfonic acid
• CAS No.: 70709-61-4
• Molecular Formula: C22H19N7O13S2
• Molecular Weight: 697.528

Synonyms:

Chemical Property of 4-methoxy-5-[(2Z)-2-{1-[(E)-(2-methoxy-4-nitro-5-sulfophenyl)diazenyl]-2-oxo-2-(phenylamino)ethylidene}hydrazino]-2-nitrobenzenesulfonic acid

Chemical Property:

• Density: 1.72g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-methoxy-5-[(2Z)-2-{1-[(E)-(2-methoxy-4-nitro-5-sulfophenyl)diazenyl]-2-oxo-2-(phenylamino)ethylidene}hydrazino]-2-nitrobenzenesulfonic acid

There total 2 articles about 4-methoxy-5-[(2Z)-2-{1-[(E)-(2-methoxy-4-nitro-5-sulfophenyl)diazenyl]-2-oxo-2-(phenylamino)ethylidene}hydrazino]-2-nitrobenzenesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

malonanilic acid (15580-32-2) + 3-diazo-4-methoxy-6-nitrobenzensulfonic acid (121451-93-2) → 3,3'-<<3-(phenylamino)carbonyl>-1,5-formazandiyl>bis(4-methoxy-6-nitro)benzenesulfonic acid disodium salt (70709-61-4)

Guidance literature:

With sodium hydroxide; In water; for 3h; Ambient temperature; pH 4.9-5.3;

Reference yield:

sodium 3,3'-<1-<(phenylamino)carbonyl>-3,4-tetrazolium>-bis(4-methoxy-6-nitro)benzenesulfonic acid (111072-31-2) → 3,3'-<<3-(phenylamino)carbonyl>-1,5-formazandiyl>bis(4-methoxy-6-nitro)benzenesulfonic acid disodium salt (70709-61-4)

Guidance literature:

With sodium hydrogencarbonate; ascorbic acid; In water; for 1.5h; Ambient temperature;

Reference yield: 27.0%

3,3'-<<3-(phenylamino)carbonyl>-1,5-formazandiyl>bis(4-methoxy-6-nitro)benzenesulfonic acid disodium salt (70709-61-4) → sodium 3,3'-<1-<(phenylamino)carbonyl>-3,4-tetrazolium>-bis(4-methoxy-6-nitro)benzenesulfonic acid (111072-31-2)

Guidance literature:

With sodium hypochlorite; In water; at 18 ℃; for 0.5h;

upstream raw materials:

malonanilic acid

3-diazo-4-methoxy-6-nitrobenzensulfonic acid

sodium 3,3'-<1-<(phenylamino)carbonyl>-3,4-tetrazolium>-bis(4-methoxy-6-nitro)benzenesulfonic acid

Downstream raw materials:

sodium 3,3'-<1-<(phenylamino)carbonyl>-3,4-tetrazolium>-bis(4-methoxy-6-nitro)benzenesulfonic acid

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