Phosphonic acid, hexadecyl-, dimethyl ester

Base Information

Chemical Name:Phosphonic acid, hexadecyl-, dimethyl ester
CAS No.:33447-06-2
Molecular Formula:C18H39O3P
Molecular Weight:334.48
Hs Code.:

Synonyms:

Suppliers and Price of Phosphonic acid, hexadecyl-, dimethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 4 raw suppliers

Chemical Property of Phosphonic acid, hexadecyl-, dimethyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Phosphonic acid, hexadecyl-, dimethyl ester

There total 1 articles about Phosphonic acid, hexadecyl-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96-36-6,868-85-9
methyl phosphite

: 544-77-4
1-iodohexadecane

: 33447-06-2
hexadecylphosphonate de dimethyle

Guidance literature:: methyl phosphite; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

1-iodohexadecane; In tetrahydrofuran; N,N-dimethyl-formamide; for 1h; Further stages.;

Reference yield:

: 33447-06-2
hexadecylphosphonate de dimethyle

: (+)-O-(n-undecyl) O-(p-nitrophenyl) hexadecylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 57 percent / oxalyl chloride / diethyl ether / 20 h / Heating

2.1: N-methylimidazole / CH₂Cl₂

3.1: N-methylimidazole / CH₂Cl₂ / 0.25 h

3.2: Daicel Chiralpack AS column

With 1-methyl-1H-imidazole; oxalyl dichloride; In diethyl ether; dichloromethane; 1.1: Chlorination / 2.1: Substitution / 3.1: Substitution / 3.2: Racemate resolution;
DOI:10.1016/S0009-3084(99)00028-6

Reference yield:

: 33447-06-2
hexadecylphosphonate de dimethyle

: (-)-O-(n-undecyl) O-(p-nitrophenyl) hexadecylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 57 percent / oxalyl chloride / diethyl ether / 20 h / Heating

2.1: N-methylimidazole / CH₂Cl₂

3.1: N-methylimidazole / CH₂Cl₂ / 0.25 h

3.2: Daicel Chiralpack AS column

With 1-methyl-1H-imidazole; oxalyl dichloride; In diethyl ether; dichloromethane; 1.1: Chlorination / 2.1: Substitution / 3.1: Substitution / 3.2: Racemate resolution;
DOI:10.1016/S0009-3084(99)00028-6