Sn(NC₅H₃(C₈H₅N)2)(C₆H₅)2

Base Information

Chemical Name:Sn(NC₅H₃(C₈H₅N)2)(C₆H₅)2
CAS No.:612838-89-8
Molecular Formula:C₃₃H₂₃N₃Sn
Molecular Weight:580.276
Hs Code.:

Sn(NC<sub>5</sub>H<sub>3</sub>(C<sub>8</sub>H<sub>5</sub>N)2)(C<sub>6</sub>H<sub>5</sub>)2

Synonyms:

Suppliers and Price of Sn(NC₅H₃(C₈H₅N)2)(C₆H₅)2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Sn(NC₅H₃(C₈H₅N)2)(C₆H₅)2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Sn(NC₅H₃(C₈H₅N)2)(C₆H₅)2

There total 1 articles about Sn(NC₅H₃(C₈H₅N)2)(C₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1135-99-5
diphenyltin(IV) dichloride

: 3882-41-5
2,6-bis(2’-indolyl)pyridine

: 612838-89-8
Sn(NC₅H₃(C₈H₅N)2)(C₆H₅)2

Guidance literature:: With n-BuLi; In tetrahydrofuran; hexane; byproducts: LiCl; under N2; ligand dissolved in Na (preheated and freshly distd. from THF); cooled to -78°C (dry ice-acetone); n-BuLi soln. in hexane addedslowly; stirred at -78°C for 40 min; THF soln. of SnCl2Ph2 added ; stirred (-78°C, 40 min); warmed to ambient temp.; stirred for 2 h; solvent removed under vac.; dissolved in CH2Cl2; filtered; anhyd. toluene layered upon filtrate; stored at ambient temp.; kept for several d; elem. anal.;
DOI:10.1021/om030404a