2-{[(4-fluorophenyl)imino]methyl}phenol

Base Information

• Chemical Name: 2-{[(4-fluorophenyl)imino]methyl}phenol
• CAS No.: 3382-62-5
• Molecular Formula: C13H10FNO
• Molecular Weight: 215.227
• Hs Code.: 2925290090
• Mol file: 3382-62-5.mol

Synonyms:N-(2-HYDROXYBENZYLIDENE)-4-FLUOROANILINE;N--4-fluor-anilin;N-<2-Hydroxy-benzyliden>-4-fluor-anilin;N-salicylaldimine-p-fluoroaniline;N-salicylidene-4-fluoroaniline;4-Fluor-N-salicyliden-anilin;4-Fluoro-N-salicylideneaniline;N-p-Fluorophenyl-salicylidenimin;

Chemical Property of 2-{[(4-fluorophenyl)imino]methyl}phenol

Chemical Property:

• Melting Point: 82.0 to 86.0 °C
• PSA: 29.10000
• LogP: 2.88960

Purity/Quality:

97% ^*data from raw suppliers

4-Fluoro-N-salicylideneaniline ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-{[(4-fluorophenyl)imino]methyl}phenol

There total 5 articles about 2-{[(4-fluorophenyl)imino]methyl}phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

salicylaldehyde (90-02-8) + 4-fluoroaniline (371-40-4) → N-salicylidene-4-fluoroaniline (3382-62-5)

Guidance literature:

With sodium sulfate; In dichloromethane; for 4h; Reflux;

DOI:10.1039/c5dt01098e

Reference yield: 95.0%

salicylaldehyde (90-02-8) + 4-fluoroaniline (371-40-4) → (E)-2-(((4-fluorophenyl)imino)methyl)phenol (3382-62-5)

Guidance literature:

In ethanol; at 20 ℃; Inert atmosphere; Schlenk technique;

DOI:10.1002/pola.27110

Reference yield:

2-methyl-benzyl alcohol (89-95-2) + 4-fluoroaniline (371-40-4) → (E)-2-(((4-fluorophenyl)imino)methyl)phenol (3382-62-5)

Guidance literature:

With hydrogenchloride; In ethanol; for 1h; pH=5; Heating;

DOI:10.1107/S0108270199008239

upstream raw materials:

salicylaldehyde

4-fluoroaniline

2-methyl-benzyl alcohol

Downstream raw materials:

C₆H₅AsO₃^(2-)*Al⁽³⁺⁾*OC₆H₄CHNC₆H₄F^(1-) = C₆H₅AsO₃Al(OC₆H₄CHNC₆H₄F)

(CH₃)3SiOAl(OC₆H₄CHNC₆H₄F)2

(C₆H₄OCHNC₆H₄F)Al(OCH(CH₃)2)2

(C₆H₄OCHNC₆H₄F)3Al

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