sodium o-allylphenolate

Base Information

• Chemical Name: sodium o-allylphenolate
• CAS No.: 3383-08-2
• Molecular Formula: C9H10O.Na
• Molecular Weight: 156.16
• Hs Code.: 2907199012
• Mol file: 3383-08-2.mol

Synonyms:Sodium o-allylphenolate;o-allylphenolate;EINECS 222-188-5;sodium 2-allylphenolate;Sodium o-allylphenoxide;2-Allyl-phenol,Natrium-Salz;2-allyl-phenol,sodium-salt;Natrium-o-allyl-phenolat;

Chemical Property of sodium o-allylphenolate

Chemical Property:

• Vapor Pressure: 0.0783mmHg at 25°C
• Boiling Point: 220oC at 760 mmHg
• Flash Point: 88.9oC
• PSA: 23.06000
• LogP: 2.55890

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of sodium o-allylphenolate

There total 1 articles about sodium o-allylphenolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

o-Allylphenol (1745-81-9) → 3-(2-hydroxyphenyl)prop-1-ene sodium salt (3383-08-2)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

Reference yield: 70.0%

1-bromo-butane (109-65-9) + 3-(2-hydroxyphenyl)prop-1-ene sodium salt (3383-08-2) → o-butoxyallylbenzene (28456-81-7)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 6h;

Reference yield: 69.0%

4-chloro-N,N-diethylbutyramide (56794-28-6) + 3-(2-hydroxyphenyl)prop-1-ene sodium salt (3383-08-2) → 4-(2-Allyl-phenoxy)-N,N-diethyl-butyramide (107770-72-9)

Guidance literature:

In tetrahydrofuran; Heating;

DOI:10.1021/jo00387a020

upstream raw materials:

o-Allylphenol

Downstream raw materials:

1-(2-allylphenoxytrimethylene)-N-pyridinium bromide

o-butoxyallylbenzene

3-(o-allyphenoxy)propanoic acid

4-(2-Allyl-phenoxy)-N,N-diethyl-butyramide

Refernces