N-hydroxy-N-phenylacrylamide

Base Information

Chemical Name:N-hydroxy-N-phenylacrylamide
CAS No.:33870-37-0
Molecular Formula:C9H9NO2
Molecular Weight:163.176
Hs Code.:
DSSTox Substance ID:DTXSID30463644
Nikkaji Number:J1.744.428J
Wikidata:Q82288627

Synonyms:N-hydroxy-N-phenylacrylamide;33870-37-0;SCHEMBL648421;DTXSID30463644;IBKOQUUOKFBMRC-UHFFFAOYSA-N

Suppliers and Price of N-hydroxy-N-phenylacrylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of N-hydroxy-N-phenylacrylamide

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:163.063328530
Heavy Atom Count:12
Complexity:173

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CC(=O)N(C1=CC=CC=C1)O

Technology Process of N-hydroxy-N-phenylacrylamide

There total 3 articles about N-hydroxy-N-phenylacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 586-96-9
Nitrosobenzene

: 107-02-8,25068-14-8
acrolein

: 33870-37-0
N-hydroxy-N-phenylacrylamide

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; 2-pentafluorophenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; In dichloromethane; at 20 ℃; for 0.166667 - 1h; Product distribution / selectivity;

Reference yield: 96.0%

: 100-65-2
N-Phenylhydroxylamine

: 814-68-6,25189-84-8
acryloyl chloride

: 33870-37-0
N-hydroxy-N-phenylacrylamide

Guidance literature:: With sodium hydrogencarbonate; In diethyl ether; water; at 0 ℃; for 0.166667h;
DOI:10.1021/ol025799t DOI:10.1021/ol0257981

Reference yield:

: 98-95-3,26969-40-4
nitrobenzene

: 33870-37-0
N-hydroxy-N-phenylacrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NH₄Cl; Zn / H₂O / 65 °C

2: 96 percent / NaHCO₃ / diethyl ether; H₂O / 0.17 h / 0 °C

With sodium hydrogencarbonate; ammonium chloride; zinc; In diethyl ether; water;
DOI:10.1021/ol025799t DOI:10.1021/ol0257981