1-(1-Bromoethyl)-2-methylbenzene

Base Information

Chemical Name:1-(1-Bromoethyl)-2-methylbenzene
CAS No.:34457-01-7
Molecular Formula:C9H11Br
Molecular Weight:199.09
Hs Code.:
DSSTox Substance ID:DTXSID101303175

Synonyms:1-(1-bromoethyl)-2-methylbenzene;34457-01-7;1-Bromoethyl-2-methylbenzene;SCHEMBL624799;DTXSID101303175;EN300-111330;A1-42138

Suppliers and Price of 1-(1-Bromoethyl)-2-methylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-(1-Bromoethyl)-2-methylbenzene

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:198.00441
Heavy Atom Count:10
Complexity:101

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=CC=C1C(C)Br

Technology Process of 1-(1-Bromoethyl)-2-methylbenzene

There total 4 articles about 1-(1-Bromoethyl)-2-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.5%

: 7287-82-3
1-O-tolyl-ethanol

: 34457-01-7
1-bromo-1-(2-methylphenyl)-ethane

Guidance literature:: With phosphorus tribromide; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 577-16-2,122382-54-1
2-Methylacetophenone

: 34457-01-7
1-bromo-1-(2-methylphenyl)-ethane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 0 - 20 °C

2: hydrogen bromide; acetic acid / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; hydrogen bromide; acetic acid; In ethanol; dichloromethane;
DOI:10.1002/anie.201604619

Reference yield:

: 529-20-4
2-methylphenyl aldehyde

: 34457-01-7
1-bromo-1-(2-methylphenyl)-ethane

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere

2: phosphorus tribromide / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With phosphorus tribromide; In diethyl ether; dichloromethane;
DOI:10.1002/anie.201902352