Silacyclohexan-4-one, 1,1-diphenyl-

Base Information

Chemical Name:Silacyclohexan-4-one, 1,1-diphenyl-
CAS No.:34564-75-5
Molecular Formula:C17H18OSi
Molecular Weight:266.415
Hs Code.:
DSSTox Substance ID:DTXSID20456303
Wikidata:Q82278682

Synonyms:Silacyclohexan-4-one, 1,1-diphenyl-;34564-75-5;SCHEMBL8034657;DTXSID20456303

Suppliers and Price of Silacyclohexan-4-one, 1,1-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silacyclohexan-4-one, 1,1-diphenyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:266.112691728
Heavy Atom Count:19
Complexity:283

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C[Si](CCC1=O)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of Silacyclohexan-4-one, 1,1-diphenyl-

There total 9 articles about Silacyclohexan-4-one, 1,1-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 17937-68-7
diphenyl-divinyl-silane

: N-cinnamyl-3-methylpyridin-2-amine

: 34564-75-5
1,1-diphenyl-1-silacyclohexan-4-one

Guidance literature:: diphenyl-divinyl-silane; N-cinnamyl-3-methylpyridin-2-amine; With chlorobis(cyclooctene)rhodium(I) dimer; tricyclohexylphosphine; In 5,5-dimethyl-1,3-cyclohexadiene; at 130 ℃; for 48h; Inert atmosphere; Sealed tube;

With hydrogenchloride; water; In 5,5-dimethyl-1,3-cyclohexadiene; at 20 ℃; for 3h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.1c04183

Reference yield: 58.0%

: 4885-02-3
Dichloromethyl methyl ether

: C₁₇H₂₁BOSi

: 34564-75-5
1,1-diphenyl-1-silacyclohexan-4-one

Guidance literature:: Dichloromethyl methyl ether; C₁₇H₂₁BOSi; With lithium tert-butoxide; In tetrahydrofuran; at 20 ℃;

With dihydrogen peroxide; sodium hydroxide; Reflux;
DOI:10.1002/anie.202115098

Reference yield:

: 17937-68-7
diphenyl-divinyl-silane

: 34564-75-5
1,1-diphenyl-1-silacyclohexan-4-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: BMS / hexane / 70 °C

1.2: 20 °C

2.1: lithium tert-butoxide / tetrahydrofuran / 20 °C

2.2: Reflux

With lithium tert-butoxide; In tetrahydrofuran; hexane;
DOI:10.1002/anie.202115098