Technology Process of Silacyclohexan-4-one, 1,1-diphenyl-
There total 9 articles about Silacyclohexan-4-one, 1,1-diphenyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
diphenyl-divinyl-silane; N-cinnamyl-3-methylpyridin-2-amine;
With
chlorobis(cyclooctene)rhodium(I) dimer; tricyclohexylphosphine;
In
5,5-dimethyl-1,3-cyclohexadiene;
at 130 ℃;
for 48h;
Inert atmosphere;
Sealed tube;
With
hydrogenchloride; water;
In
5,5-dimethyl-1,3-cyclohexadiene;
at 20 ℃;
for 3h;
Inert atmosphere;
Sealed tube;
DOI:10.1021/acs.orglett.1c04183
- Guidance literature:
-
Dichloromethyl methyl ether; C17H21BOSi;
With
lithium tert-butoxide;
In
tetrahydrofuran;
at 20 ℃;
With
dihydrogen peroxide; sodium hydroxide;
Reflux;
DOI:10.1002/anie.202115098
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: BMS / hexane / 70 °C
1.2: 20 °C
2.1: lithium tert-butoxide / tetrahydrofuran / 20 °C
2.2: Reflux
With
lithium tert-butoxide;
In
tetrahydrofuran; hexane;
DOI:10.1002/anie.202115098
