4-methyl-N-(3-methylpyridin-2-yl)benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-(3-methylpyridin-2-yl)benzenesulfonamide
CAS No.:346696-65-9
Molecular Formula:C₁₃H₁₄N₂O₂S
Molecular Weight:262.332
Hs Code.:
DSSTox Substance ID:DTXSID70403069
Nikkaji Number:J1.874.861D
Wikidata:Q82206617
Mol file:346696-65-9.mol

Synonyms:346696-65-9;2-(Tosylamino)-3-methylpyridine;4-methyl-N-(3-methylpyridin-2-yl)benzenesulfonamide;Benzenesulfonamide, 4-methyl-N-(3-methyl-2-pyridinyl)-;AG-205/03194024;Oprea1_376319;4-methyl-N-(3-methyl-2-pyridinyl)benzenesulfonamide;DTXSID70403069;AKOS003829612;AB00042037-01

Suppliers and Price of 4-methyl-N-(3-methylpyridin-2-yl)benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 4-methyl-N-(3-methylpyridin-2-yl)benzenesulfonamide

Chemical Property:

PSA：67.44000
LogP:3.65300
XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:262.07759887
Heavy Atom Count:18
Complexity:356

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NC2=C(C=CC=N2)C

Technology Process of 4-methyl-N-(3-methylpyridin-2-yl)benzenesulfonamide

There total 1 articles about 4-methyl-N-(3-methylpyridin-2-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.7%

: 1603-40-3
3-methylpyridin-2-ylamine

: 98-59-9
p-toluenesulfonyl chloride

: 346696-65-9
N-(3-methyl-2-pyridyl)-p-toluenesulfonamide

Guidance literature:: With sodium carbonate; In dichloromethane;
DOI:10.1002/ejic.200300338

Reference yield:

: 7732-18-5
water

: 12775-96-1,15158-11-9,15721-63-8,16941-75-6,17493-86-6,19498-52-3,20499-83-6,20499-84-7,20499-85-8,20499-86-9,20573-10-8,20573-11-9,21595-51-7,21595-52-8,22206-52-6,26445-28-3,28959-95-7,37362-93-9,39417-05-5,54603-16-6,54603-23-5,54603-32-6,54603-40-6,54603-48-4,54603-81-5,54603-89-3,56316-56-4,95985-91-4,122297-32-9,7440-50-8
copper

: 346696-65-9
N-(3-methyl-2-pyridyl)-p-toluenesulfonamide

: [copper(II)(N-(3-methyl-2-pyridyl)-p-toluenesulfonamide^(1-))2(H₂O)]

Guidance literature:: With tetraethylammonium perchlorate; In acetonitrile; Electrochem. Process; copper anode in ligand soln. (TEAP electrolyte, 12 V, 10 mA for 1 h); elem. anal.;
DOI:10.1002/ejic.200300338

Reference yield:

: 366-18-7
[2,2]bipyridinyl

: 12775-96-1,15158-11-9,15721-63-8,16941-75-6,17493-86-6,19498-52-3,20499-83-6,20499-84-7,20499-85-8,20499-86-9,20573-10-8,20573-11-9,21595-51-7,21595-52-8,22206-52-6,26445-28-3,28959-95-7,37362-93-9,39417-05-5,54603-16-6,54603-23-5,54603-32-6,54603-40-6,54603-48-4,54603-81-5,54603-89-3,56316-56-4,95985-91-4,122297-32-9,7440-50-8
copper

: 346696-65-9
N-(3-methyl-2-pyridyl)-p-toluenesulfonamide

: [copper(II)(N-(3-methyl-2-pyridyl)-p-toluenesulfonamide^(1-))2(2,2'-bipyridine)]

Guidance literature:: With tetraethylammonium perchlorate; In acetonitrile; Electrochem. Process; copper anode in ligand and bipy soln. (0.75:0.37 molar ratio) (TEAP electrolyte, 10 V, 10 mA for 1 h); elem. anal.;
DOI:10.1002/ejic.200300338