2H-Pyran, tetrahydro-2-[[18-(4-iodophenyl)octadecyl]oxy]-

Base Information

Chemical Name:2H-Pyran, tetrahydro-2-[[18-(4-iodophenyl)octadecyl]oxy]-
CAS No.:347143-82-2
Molecular Formula:C29H49IO2
Molecular Weight:556.611
Hs Code.:
DSSTox Substance ID:DTXSID30470777
Mol file:347143-82-2.mol

Synonyms:347143-82-2;2-((18-(4-Iodophenyl)octadecyl)oxy)tetrahydro-2H-pyran;2H-Pyran, tetrahydro-2-[[18-(4-iodophenyl)octadecyl]oxy]-;SCHEMBL13387441;DTXSID30470777

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Chemical Property of 2H-Pyran, tetrahydro-2-[[18-(4-iodophenyl)octadecyl]oxy]-

Chemical Property:

XLogP3:11.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:20
Exact Mass:556.27773
Heavy Atom Count:32
Complexity:395

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCOC(C1)OCCCCCCCCCCCCCCCCCCC2=CC=C(C=C2)I

Technology Process of 2H-Pyran, tetrahydro-2-[[18-(4-iodophenyl)octadecyl]oxy]-

There total 9 articles about 2H-Pyran, tetrahydro-2-[[18-(4-iodophenyl)octadecyl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 873301-57-6
12-(p-iodophenyl)dodecyl tosylate

: 53963-10-3
2-[(6-bromohexyl)oxy]tetrahydro-2H-pyran

: 347143-82-2
tetrahydro-2-[18-(p-iodophenyl)octadecyloxy]-2H-pyran

Guidance literature:: 2-[(6-bromohexyl)oxy]tetrahydro-2H-pyran; With magnesium; In tetrahydrofuran; at 20 ℃;

With dilithium tetrachlorocuprate; In tetrahydrofuran; at -78 ℃;

12-(p-iodophenyl)dodecyl tosylate; In tetrahydrofuran; at -78 - 20 ℃; for 15h;
DOI:10.1021/jm050252g

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 347143-82-2
tetrahydro-2-[18-(p-iodophenyl)octadecyloxy]-2H-pyran

Guidance literature:: Multi-step reaction with 2 steps

1.1: 92 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 5 h / 20 °C

2.1: Mg / tetrahydrofuran / 20 °C

2.2: Li₂CuCl₄ / tetrahydrofuran / -78 °C

2.3: 64 percent / tetrahydrofuran / 15 h / -78 - 20 °C

With pyridinium p-toluenesulfonate; magnesium; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm050252g

Reference yield:

: 167634-94-8
12-(p-iodophenyl)dodecanol

: 347143-82-2
tetrahydro-2-[18-(p-iodophenyl)octadecyloxy]-2H-pyran

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96 percent / N,N-(dimethylamino)pyridine / CH₂Cl₂ / 16 h

2.1: Mg / tetrahydrofuran / 20 °C

2.2: Li₂CuCl₄ / tetrahydrofuran / -78 °C

2.3: 64 percent / tetrahydrofuran / 15 h / -78 - 20 °C

With dmap; magnesium; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm050252g