Tert-butyl 4-bromo-3-methylbenzoate

Base Information

Chemical Name:Tert-butyl 4-bromo-3-methylbenzoate
CAS No.:347174-28-1
Molecular Formula:C12H15BrO2
Molecular Weight:271.154
Hs Code.:2916399090
DSSTox Substance ID:DTXSID50474358
Wikidata:Q82304337
Mol file:347174-28-1.mol

Synonyms:TERT-BUTYL 4-BROMO-3-METHYLBENZOATE;347174-28-1;4-Bromo-3-methylbenzoic acid tert-butyl ester;TERT-BUTYL4-BROMO-3-METHYLBENZOATE;4-Bromo-3-methyl-benzoic Acid Tert-Butyl Ester;SCHEMBL1132147;DTXSID50474358;RIHBTHGKWXRWQX-UHFFFAOYSA-N;XNA17428;tert butyl 4-bromo-3-methylbenzoate;AB8582;MFCD08703429;AKOS027327240;AS-44895;CS-0195357;EN300-332357;A854327;A1-04194

Suppliers and Price of Tert-butyl 4-bromo-3-methylbenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
tert-Butyl4-Bromo-3-methylbenzoate
100mg
$ 60.00

Matrix Scientific
4-Bromo-3-methylbenzoic acid tert-butyl ester 95%
10g
$ 908.00

Matrix Scientific
4-Bromo-3-methylbenzoic acid tert-butyl ester 95%
25g
$ 1650.00

Labseeker
tert-butyl4-bromo-3-methylbenzoate 95
200g
$ 1833.00

Crysdot
tert-Butyl4-bromo-3-methylbenzoate 95+%
25g
$ 1485.00

Crysdot
tert-Butyl4-bromo-3-methylbenzoate 95+%
5g
$ 424.00

Crysdot
tert-Butyl4-bromo-3-methylbenzoate 95+%
10g
$ 762.00

AOBChem
tert-Butyl4-bromo-3-methylbenzoate 95%
5g
$ 430.00

American Custom Chemicals Corporation
TERT-BUTYL-4-BROMO-3-METHYLBENZOATE 95.00%
5MG
$ 505.93

AK Scientific
tert-Butyl4-bromo-3-methylbenzoate
5g
$ 651.00

Total 18 raw suppliers

Chemical Property of Tert-butyl 4-bromo-3-methylbenzoate

Chemical Property:

Boiling Point:320.7±22.0 °C(Predicted)
PSA：26.30000
Density:1.295±0.06 g/cm3(Predicted)
LogP:3.71280
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:270.02554
Heavy Atom Count:15
Complexity:232

Purity/Quality:

99%, ^*data from raw suppliers

tert-Butyl4-Bromo-3-methylbenzoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC(=C1)C(=O)OC(C)(C)C)Br

Technology Process of Tert-butyl 4-bromo-3-methylbenzoate

There total 7 articles about Tert-butyl 4-bromo-3-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 347174-28-1
tert-butyl 4-bromo-3-methylbenzoate

Guidance literature:: In tetrahydrofuran; n-heptane; ethyl acetate;

Reference yield: 87.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 7697-28-1
4-bromo-3-methylbenzoic acid

: 347174-28-1
tert-butyl 4-bromo-3-methylbenzoate

Guidance literature:: With dmap; In tetrahydrofuran; Reflux;

Reference yield: 86.0%

: 7697-28-1
4-bromo-3-methylbenzoic acid

: 865-47-4
potassium tert-butylate

: 347174-28-1
tert-butyl 4-bromo-3-methylbenzoate

Guidance literature:: 4-bromo-3-methylbenzoic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 2.33333h;

potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; for 1h;