2a,3-dibenzyl-2a,3-dihydrodicyclopentaheptalene

Base Information

• Chemical Name: 2a,3-dibenzyl-2a,3-dihydrodicyclopentaheptalene
• CAS No.: 139914-67-3
• Molecular Formula: C₃₀H₂₄
• Molecular Weight: 384.521

Synonyms:

Chemical Property of 2a,3-dibenzyl-2a,3-dihydrodicyclopentaheptalene

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2a,3-dibenzyl-2a,3-dihydrodicyclopentaheptalene

There total 3 articles about 2a,3-dibenzyl-2a,3-dihydrodicyclopentaheptalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

azupyrene (193-85-1) + benzyl mesylate (55791-06-5) → 2a,3-dibenzyl-2a,3-dihydrodicyclopentaheptalene (139914-67-3) + trans-15,16-dibenzyl-1,4,8,11-ethanediylidene<14>annulene (139914-62-8)

Guidance literature:

With lithium; Multistep reaction; 1. THF, -30 deg C, 2.) THF, 20 deg C, 15 min;

Reference yield:

azupyrene (193-85-1) + benzyl bromide (100-39-0) → 2a,3-dibenzyl-2a,3-dihydrodicyclopentaheptalene (139914-67-3) + trans-15,16-dibenzyl-1,4,8,11-ethanediylidene<14>annulene (139914-62-8)

Guidance literature:

With lithium; Multistep reaction; 1. THF, -30 deg C, 2.) THF, 20 deg C, 15 min;

Reference yield:

azupyrene (193-85-1) + benzyl chloride (100-44-7) → 2a,3-dibenzyl-2a,3-dihydrodicyclopentaheptalene (139914-67-3) + trans-15,16-dibenzyl-1,4,8,11-ethanediylidene<14>annulene (139914-62-8)

Guidance literature:

With lithium; Multistep reaction; 1. THF, -30 deg C, 2.) THF, 20 deg C, 15 min;

upstream raw materials:

azupyrene

benzyl mesylate

benzyl bromide

benzyl chloride

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