Benzenamine, 2,2'-dithiobis[N-methyl-

Base Information

• Chemical Name: Benzenamine, 2,2'-dithiobis[N-methyl-
• CAS No.: 3495-63-4
• Molecular Formula: C14H16N2S2
• Molecular Weight: 276.426
• DSSTox Substance ID: DTXSID80395461
• Nikkaji Number: J802.565G
• Wikidata: Q82195572
• Mol file: 3495-63-4.mol

Synonyms:3495-63-4;Benzenamine, 2,2'-dithiobis[N-methyl-;SCHEMBL8897003;DTXSID80395461;bis(o-methylamino-phenyl) disulfide;2,2'-Dithiobis(N-methylbenzenamine)

Chemical Property of Benzenamine, 2,2'-dithiobis[N-methyl-

Chemical Property:

• XLogP3: 4.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 276.07549087
• Heavy Atom Count: 18
• Complexity: 214

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CNC1=CC=CC=C1SSC2=CC=CC=C2NC

Technology Process of Benzenamine, 2,2'-dithiobis[N-methyl-

There total 19 articles about Benzenamine, 2,2'-dithiobis[N-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

2-amino-3-methylbenzo[d]thiazol-3-ium iodide → 2,2'-dithiobis(N-methylaniline) (3495-63-4)

Guidance literature:

With potassium hydroxide; In water; for 14h; Reflux;

DOI:10.1002/anie.201901320

Reference yield:

2-(methylamino)benzenethiol (21749-63-3) → 2,2'-dithiobis(N-methylaniline) (3495-63-4)

Guidance literature:

With dimethyl sulfoxide; at 80 - 90 ℃; for 8h;

Reference yield:

3-methylbenzothiazolenitrosoimine (19617-04-0) → 2,2'-dithiobis(N-methylaniline) (3495-63-4)

Guidance literature:

With sec-butylmagnesium bromide; In diethyl ether;

DOI:10.1246/bcsj.48.3270

upstream raw materials:

3-methylbenzothiazolenitrosoimine

bis<2-(N-formyl-N-methylamino)phenyl> disulfide

2-(2-Methylamino-phenylsulfinyl)-11-methyl-cycloundecanon

ethyl bromoacetate

Downstream raw materials:

bis<2-(N-formyl-N-methylamino)phenyl> disulfide

N-{2-[2-(acetylmethylamino)phenyldisulfanyl]phenyl}-N-methylacetamide

6,7,8,9,10,11,12,13,14,15-decahydro-4-methyl-2,3-benzo-1-thia-4-azacyclopentadecen-5-one

9-Bromo-nonanoic acid (2-{2-[(9-bromo-nonanoyl)-methyl-amino]-phenyldisulfanyl}-phenyl)-methyl-amide