9-Bromo-nonanoic acid (2-{2-[(9-bromo-nonanoyl)-methyl-amino]-phenyldisulfanyl}-phenyl)-methyl-amide

Base Information

Chemical Name:9-Bromo-nonanoic acid (2-{2-[(9-bromo-nonanoyl)-methyl-amino]-phenyldisulfanyl}-phenyl)-methyl-amide
CAS No.:78082-11-8
Molecular Formula:C₃₂H₄₆Br₂N₂O₂S₂
Molecular Weight:714.669
Hs Code.:

Synonyms:9-Bromo-nonanoic acid (2-{2-[(9-bromo-nonanoyl)-methyl-amino]-phenyldisulfanyl}-phenyl)-methyl-amide

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Chemical Property of 9-Bromo-nonanoic acid (2-{2-[(9-bromo-nonanoyl)-methyl-amino]-phenyldisulfanyl}-phenyl)-methyl-amide

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Technology Process of 9-Bromo-nonanoic acid (2-{2-[(9-bromo-nonanoyl)-methyl-amino]-phenyldisulfanyl}-phenyl)-methyl-amide

There total 8 articles about 9-Bromo-nonanoic acid (2-{2-[(9-bromo-nonanoyl)-methyl-amino]-phenyldisulfanyl}-phenyl)-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.5%

: 73674-10-9
9-bromononanoyl chloride

: 3495-63-4
2,2'-dithiobis(N-methylaniline)

: 78082-11-8
9-Bromo-nonanoic acid (2-{2-[(9-bromo-nonanoyl)-methyl-amino]-phenyldisulfanyl}-phenyl)-methyl-amide

Guidance literature:: With triethylamine; In diethyl ether; for 0.5h; Ambient temperature;

Reference yield:

: 73674-30-3
2-(2-Methylamino-phenylsulfinyl)-11-methyl-cycloundecanon

: 78082-11-8
9-Bromo-nonanoic acid (2-{2-[(9-bromo-nonanoyl)-methyl-amino]-phenyldisulfanyl}-phenyl)-methyl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: xylene / 2 h / 100 °C

2: 79.5 percent / Et₃N / diethyl ether / 0.5 h / Ambient temperature

With triethylamine; In diethyl ether; xylene;

Reference yield:

: 77922-74-8
15,17-Dimethyl-6,7,8,9,10,11,12,13,14,15-decahydro-17H-5-thia-17-aza-benzocyclopentadecen-16-one

: 78082-11-8
9-Bromo-nonanoic acid (2-{2-[(9-bromo-nonanoyl)-methyl-amino]-phenyldisulfanyl}-phenyl)-methyl-amide

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / NaIO₄ / H₂O; methanol / 20 h / Ambient temperature

2: LDA / tetrahydrofuran / 1.) -78 deg C, 30 min, 2.) 30 min, ice bath

3: xylene / 2 h / 100 °C

4: 79.5 percent / Et₃N / diethyl ether / 0.5 h / Ambient temperature

With sodium periodate; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; water; xylene;