Ethanol, 2-[[(4-chlorophenyl)methyl]methylamino]-

Base Information

• Chemical Name: Ethanol, 2-[[(4-chlorophenyl)methyl]methylamino]-
• CAS No.: 35113-60-1
• Molecular Formula: C10H14ClNO
• Molecular Weight: 199.67700
• Mol file: 35113-60-1.mol

Synonyms:Methyl-<2-hydroxy-aethyl>-<4-chlor-benzyl>-amin;2-[(4-Chloro-benzyl)-methyl-amino]-ethanol;N-p-Chlorbenzyl-N-methylaminoethanol;N-(4-chlorobenzyl)-N-methylethanolamine;

Chemical Property of Ethanol, 2-[[(4-chlorophenyl)methyl]methylamino]-

Chemical Property:

• PSA: 23.47000
• LogP: 1.76410

Purity/Quality:

99% ^*data from raw suppliers

2-((4-Chlorobenzyl)(methyl)amino)ethanol 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ethanol, 2-[[(4-chlorophenyl)methyl]methylamino]-

There total 2 articles about Ethanol, 2-[[(4-chlorophenyl)methyl]methylamino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

(2-hydroxyethyl)(methyl)amine (109-83-1) + 1-Chloro-4-(chloromethyl)benzene (104-83-6) → N-hydroxyethyl-4-chlorobenzyl-N-methylamine (35113-60-1)

Guidance literature:

In xylene; for 7h; Heating;

DOI:10.1021/jm00161a022

Reference yield:

→ N-hydroxyethyl-4-chlorobenzyl-N-methylamine (35113-60-1)

Guidance literature:

Methyl-<4-chlor-benzyl>-amin, Aethylenchlorhydrin;

DOI:10.1021/jo01067a075

Reference yield: 95.0%

N-hydroxyethyl-4-chlorobenzyl-N-methylamine (35113-60-1) → 1-chloro-3-(4-chlorobenzyl)-3-azabutane hydrochloride (23510-20-5)

Guidance literature:

With thionyl chloride; In chloroform; 1.) RT, overnight, 2.) reflux, 2 h;

DOI:10.1021/jm00161a022

upstream raw materials:

(2-hydroxyethyl)(methyl)amine

1-Chloro-4-(chloromethyl)benzene

Downstream raw materials:

2-[N-(4-chlorobenzyl)-N-methylamino]-ethyl acetoacetate

1-chloro-3-(4-chlorobenzyl)-3-azabutane hydrochloride

2-(4-chlorobenzyl)-2,5-diazahexane

6-<<7-(4-chlorobenzyl)-4-methyl-4,7-diazooctan-1-yl>oxy>-5-methyl<1>benzopyrano<2,3-d>-1,2,3-triazol-9(1H)-one trifluoroacetate

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