3,4,5-Tribromo-2-(2,4-dibromophenoxy)phenol

Base Information

Chemical Name:3,4,5-Tribromo-2-(2,4-dibromophenoxy)phenol
CAS No.:35162-01-7
Molecular Formula:C12H5Br5O2
Molecular Weight:580.69
Hs Code.:2909500000
UNII:B1LB95ZSV8
ChEMBL ID:CHEMBL464577
DSSTox Substance ID:DTXSID60474586
Metabolomics Workbench ID:136591
Nikkaji Number:J107.383D
Wikidata:Q27136826
Mol file:35162-01-7.mol

Synonyms:3,4,5-tribromo-2-(2,4-dibromophenoxy)phenol;35162-01-7;B1LB95ZSV8;6-OH-Bde 85;UNII-B1LB95ZSV8;Phenol, 3,4,5-tribromo-2-(2,4-dibromophenoxy)-;CHEMBL464577;CHEBI:68326;6-Hydroxy-2,2',3,4,4'-pentabromodiphenylether;2-(2,4-Bis(bromanyl)phenoxy)-3,4,5-tris(bromanyl)phenol;6-hydroxy-2,2',3,4,4'-pentabromodiphenyl ether;SCHEMBL5527228;DTXSID60474586;BDBM50292443;PD181084;NS00077078;3,4,5-tribromo-2-(2',4'-dibromophenoxy)phenol;3,4,5-Tribromo-2-(2',4'-dibromo-phenoxy)-phenol;Q27136826;3,4,5-tribromo-2-(2'', 4''-dibromo-phenoxy)phenol

Suppliers and Price of 3,4,5-Tribromo-2-(2,4-dibromophenoxy)phenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3,4,5-Tribromo-2-(2,4-dibromophenoxy)phenol

Chemical Property:

PSA：29.46000
LogP:6.99700
XLogP3:6.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:579.61654
Heavy Atom Count:19
Complexity:306

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C=C1Br)Br)OC2=C(C(=C(C=C2O)Br)Br)Br

Technology Process of 3,4,5-Tribromo-2-(2,4-dibromophenoxy)phenol

There total 7 articles about 3,4,5-Tribromo-2-(2,4-dibromophenoxy)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 38926-88-4
1,2,3-tribromo-4-(2,4-dibromophenoxy)-5-methoxybenzene

: 35162-01-7
6-hydroxy-2,2′,3,4,4′-pentabromodiphenyl ether

Guidance literature:: With boron tribromide; In dichloromethane; at 50 ℃; for 36h;
DOI:10.1002/ejoc.200300081

Reference yield:

: 615-57-6
2,4-dibromo-aniline

: 35162-01-7
6-hydroxy-2,2′,3,4,4′-pentabromodiphenyl ether

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; sodium nitrite; potassium iodide / 0 - 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / acetonitrile / 0.83 h / 55 °C

2.2: 0.25 h / 55 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / 0 °C

3.2: 47 h / 40 °C

4.1: boron tribromide / 49 h / 0 - 20 °C

With hydrogenchloride; potassium tert-butylate; boron tribromide; 3-chloro-benzenecarboperoxoic acid; potassium iodide; sodium nitrite; In tetrahydrofuran; acetonitrile;
DOI:10.1021/acs.joc.1c01214

Reference yield:

: (2,4-dibromophenyl)(2,4,6-trimethoxyphenyl)iodonium tosylate

: 35162-01-7
6-hydroxy-2,2′,3,4,4′-pentabromodiphenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / 0 °C

1.2: 47 h / 40 °C

2.1: boron tribromide / 49 h / 0 - 20 °C

With potassium tert-butylate; boron tribromide; In tetrahydrofuran;
DOI:10.1021/acs.joc.1c01214