Acetic acid, [[3-[2-chloro-5-[3,6-dihydro-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidin yl]-4-fluorophenoxy]-2-pyridinyl]oxy]-, methyl ester

Base Information

• Chemical Name: Acetic acid, [[3-[2-chloro-5-[3,6-dihydro-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidin yl]-4-fluorophenoxy]-2-pyridinyl]oxy]-, methyl ester
• CAS No.: 353292-72-5
• Molecular Formula: C19H12ClF4N3O6
• Molecular Weight: 489.767
• Mol file: 353292-72-5.mol

Synonyms:

Chemical Property of Acetic acid, [[3-[2-chloro-5-[3,6-dihydro-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidin yl]-4-fluorophenoxy]-2-pyridinyl]oxy]-, methyl ester

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Technology Process of Acetic acid, [[3-[2-chloro-5-[3,6-dihydro-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidin yl]-4-fluorophenoxy]-2-pyridinyl]oxy]-, methyl ester

There total 3 articles about Acetic acid, [[3-[2-chloro-5-[3,6-dihydro-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidin yl]-4-fluorophenoxy]-2-pyridinyl]oxy]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}phenyl]trifluoroacetoacetamide (477716-64-6) → 3-{2-chloro-4-fluoro-5-[2,6-dioxo-4-(trifluoromethyl)-1,2,3,6-tetrahydropyrimidin-1-yl]phenoxy}-2-(methoxycarbonyl)methoxypyridine (353292-72-5)

Guidance literature:

With acetic acid; In water;

Reference yield:

N-[4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}phenyl]trifluoroacetoacetamide (477716-64-6) + sodium isocyanate (917-61-3) → 3-{2-chloro-4-fluoro-5-[2,6-dioxo-4-(trifluoromethyl)-1,2,3,6-tetrahydropyrimidin-1-yl]phenoxy}-2-(methoxycarbonyl)methoxypyridine (353292-72-5)

Guidance literature:

With acetic acid; at 50 - 110 ℃; for 2.5h;

Reference yield:

4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}phenyl isocyanate (353292-61-2) + ethyl 3-amino-4,4,4-trifluorocrotonate (141860-78-8) → 3-{2-chloro-4-fluoro-5-[2,6-dioxo-4-(trifluoromethyl)-1,2,3,6-tetrahydropyrimidin-1-yl]phenoxy}-2-(methoxycarbonyl)methoxypyridine (353292-72-5)

Guidance literature:

In hydrogenchloride; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; N,N-dimethyl-formamide;

upstream raw materials:

N-[4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}phenyl]trifluoroacetoacetamide

sodium isocyanate

4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}phenyl isocyanate

ethyl 3-amino-4,4,4-trifluorocrotonate

Downstream raw materials:

methyl 2-((3-(2-chloro-4-fluoro-5-(3-methyl-2,6-dioxo-4-(trifluoromethyl)-2,3-dihydropyrimidin-1(6H)-yl)phenoxy)pyridin-2-yl)oxy)acetate

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