4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}phenyl isocyanate

Base Information

• Chemical Name: 4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}phenyl isocyanate
• CAS No.: 353292-61-2
• Molecular Formula: C₁₅H₁₀ClFN₂O₅
• Molecular Weight: 352.706

Synonyms:4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}phenyl isocyanate

Chemical Property of 4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}phenyl isocyanate

Chemical Property:

Purity/Quality:

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Technology Process of 4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}phenyl isocyanate

There total 1 articles about 4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}phenyl isocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}aniline (353292-53-2) + bis(trichloromethyl) carbonate (32315-10-9) → 4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}phenyl isocyanate (353292-61-2)

Guidance literature:

With triethylamine; In ethyl acetate;

Reference yield:

4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}phenyl isocyanate (353292-61-2) + ethyl 3-amino-4,4,4-trifluorocrotonate (141860-78-8) → 3-{2-chloro-4-fluoro-5-[2,6-dioxo-4-(trifluoromethyl)-1,2,3,6-tetrahydropyrimidin-1-yl]phenoxy}-2-(methoxycarbonyl)methoxypyridine (353292-72-5)

Guidance literature:

In hydrogenchloride; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; N,N-dimethyl-formamide;

upstream raw materials:

4-chloro-2-fluoro-5-{2-(methoxycarbonyl)methoxy-pyridin-3-yloxy}aniline

bis(trichloromethyl) carbonate

Downstream raw materials:

3-{2-chloro-4-fluoro-5-[2,6-dioxo-4-(trifluoromethyl)-1,2,3,6-tetrahydropyrimidin-1-yl]phenoxy}-2-(methoxycarbonyl)methoxypyridine

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