1-Nitro-2-[(phenylselanyl)methyl]benzene

Base Information

Chemical Name:1-Nitro-2-[(phenylselanyl)methyl]benzene
CAS No.:3541-43-3
Molecular Formula:C13H11NO2Se
Molecular Weight:292.196
Hs Code.:
DSSTox Substance ID:DTXSID20549784
Wikidata:Q82428922
Mol file:3541-43-3.mol

Synonyms:3541-43-3;1-Nitro-2-[(phenylselanyl)methyl]benzene;DTXSID20549784

Suppliers and Price of 1-Nitro-2-[(phenylselanyl)methyl]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Nitro-2-[(phenylselanyl)methyl]benzene

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:292.99550
Heavy Atom Count:17
Complexity:248

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)[Se]CC2=CC=CC=C2[N+](=O)[O-]

Technology Process of 1-Nitro-2-[(phenylselanyl)methyl]benzene

There total 4 articles about 1-Nitro-2-[(phenylselanyl)methyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 68819-94-3
p-tolyl benzeneselenosulfonate

: 23308-83-0
(2-nitrobenzyl)triphenylphosphonium bromide

: 3541-43-3
o-Nitro-benzyl-phenyl-selenid

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 0.5h;
DOI:10.1021/acs.joc.1c00114

Reference yield:

: 1666-13-3
diphenyl diselenide

: 3958-60-9
2-nitrophenylmethyl bromide

: 3541-43-3
o-Nitro-benzyl-phenyl-selenid

Guidance literature:: diphenyl diselenide; With sodium tetrahydroborate; In ethanol; Inert atmosphere;

2-nitrophenylmethyl bromide; In ethanol; for 3h; Reflux; Inert atmosphere;
DOI:10.1016/j.tetlet.2016.08.073

Reference yield:

: 1666-13-3
diphenyl diselenide

: 3541-43-3
o-Nitro-benzyl-phenyl-selenid

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / acetonitrile / 2 h

2: triethylamine / dichloromethane / 0.5 h / 25 °C

With N-Bromosuccinimide; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/acs.joc.1c00114