4-methyl-N'-[(E,2E)-1-methyl-3-phenyl-2-propenylidene]benzenesulfonohydrazide

Base Information

Chemical Name:4-methyl-N'-[(E,2E)-1-methyl-3-phenyl-2-propenylidene]benzenesulfonohydrazide
CAS No.:17336-65-1
Molecular Formula:C17H18 N2 O2 S
Molecular Weight:314.408
Hs Code.:
NSC Number:333418
DSSTox Substance ID:DTXSID40430660

Synonyms:NSC333418;17336-65-1;DTXSID40430660;AKOS024344428;NSC-333418;4-methyl-N'-[(E,2E)-1-methyl-3-phenyl-2-propenylidene]benzenesulfonohydrazide

Suppliers and Price of 4-methyl-N'-[(E,2E)-1-methyl-3-phenyl-2-propenylidene]benzenesulfonohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 4-methyl-N'-[(E,2E)-1-methyl-3-phenyl-2-propenylidene]benzenesulfonohydrazide

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:314.10889899
Heavy Atom Count:22
Complexity:491

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NN=C(C)C=CC2=CC=CC=C2
Isomeric SMILES:CC1=CC=C(C=C1)S(=O)(=O)N/N=C(\C)/C=C/C2=CC=CC=C2

Technology Process of 4-methyl-N'-[(E,2E)-1-methyl-3-phenyl-2-propenylidene]benzenesulfonohydrazide

There total 4 articles about 4-methyl-N'-[(E,2E)-1-methyl-3-phenyl-2-propenylidene]benzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 122-57-6
1-Phenylbut-1-en-3-one

: 17336-65-1
4-phenylbut-3-en-2-one p-tosylhydrazone

Guidance literature:: With hydrogenchloride; In methanol;
DOI:10.1246/bcsj.44.1885

Reference yield:

: 100-52-7
benzaldehyde

: 17336-65-1
4-phenylbut-3-en-2-one p-tosylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; water / 0.08 h / 20 °C / Inert atmosphere

2: methanol / 60 °C / Inert atmosphere

In methanol; ethanol; water;
DOI:10.1021/acs.orglett.7b00213

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 17336-65-1
4-phenylbut-3-en-2-one p-tosylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrabutyl-ammonium chloride; sodium hydrogencarbonate / N,N-dimethyl-formamide / 4 h / 100 °C / Microwave irradiation; Inert atmosphere

2: sulfuric acid / 1.5 h / 80 °C / Microwave irradiation

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sulfuric acid; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; In N,N-dimethyl-formamide; 1: |Heck Reaction;
DOI:10.1002/ejoc.202000066