1-tert-butyl 6-Methyl 1H-indole-1,6-dicarboxylate

Base Information

• Chemical Name: 1-tert-butyl 6-Methyl 1H-indole-1,6-dicarboxylate
• CAS No.: 354587-63-6
• Molecular Formula: C₁₅H₁₇NO₄
• Molecular Weight: 275.304
• Mol file: 354587-63-6.mol

Synonyms:1H-Indole-1,6-dicarboxylic acid, 1-(1,1-dimethylethyl) 6-methyl ester;

Chemical Property of 1-tert-butyl 6-Methyl 1H-indole-1,6-dicarboxylate

Chemical Property:

• PSA: 57.53000
• LogP: 3.21110
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

O1-tert-ButylO6-MethylIndole-1,6-dicarboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-tert-butyl 6-Methyl 1H-indole-1,6-dicarboxylate

There total 5 articles about 1-tert-butyl 6-Methyl 1H-indole-1,6-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

indole-6-carboxylic acid methyl ester (50820-65-0) + di-tert-butyl dicarbonate (24424-99-5) → indole-1,6-dicarboxylic acid 1-tert-butyl ester 6-methyl ester (354587-63-6)

Guidance literature:

dmap; In tetrahydrofuran; at 20 ℃; for 2.33333h;

Reference yield: 95.0%

di-tert-butyl dicarbonate (24424-99-5) + methyl 1H-indole-1,6-dicarboxylate → indole-1,6-dicarboxylic acid 1-tert-butyl ester 6-methyl ester (354587-63-6)

Guidance literature:

With dmap; In acetonitrile; at 20 ℃;

Reference yield: 70.0%

tert-butyl carbazate (4248-19-5) + 3-bromo-4-(2-bromovinyl)benzoic acid methyl ester (1129606-97-8) → indole-1,6-dicarboxylic acid 1-tert-butyl ester 6-methyl ester (354587-63-6)

Guidance literature:

With potassium phosphate; copper (I) acetate; N,N`-dimethylethylenediamine; In toluene; at 110 ℃; for 24h; Inert atmosphere;

DOI:10.1039/b817254d

upstream raw materials:

indole-6-carboxylic acid methyl ester

di-tert-butyl dicarbonate

tert-butyl carbazate

3-bromo-4-(2-bromovinyl)benzoic acid methyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 354587-63-6 1-tert-butyl 6-Methyl 1H-indole-1,6-dicarboxylate

Send

Send

Metric Ton KG G Pound L ML

Send

Send