Benzyl 2,2-diethoxyethylcarbamate

Base Information

Chemical Name:Benzyl 2,2-diethoxyethylcarbamate
CAS No.:60085-61-2
Molecular Formula:C14H21NO4
Molecular Weight:267.325
Hs Code.:2924299090
NSC Number:158340
DSSTox Substance ID:DTXSID70303439
Nikkaji Number:J1.918.102B
Wikidata:Q82048730
Mol file:60085-61-2.mol

Synonyms:60085-61-2;BENZYL 2,2-DIETHOXYETHYLCARBAMATE;benzyl N-(2,2-diethoxyethyl)carbamate;Benzyl (2,2-diethoxyethyl)carbamate;(2,2-Diethoxy-ethyl)-carbamic acid benzyl ester;benzyl(2,2-diethoxyethyl)carbamate;NSC158340;N-Cbz-2,2-diethoxyethylamine;SCHEMBL5740648;DTXSID70303439;YBQUFRCXCFAQQM-UHFFFAOYSA-N;benzyl 2,2-diethoxyethyl carbamate;MFCD00087219;AKOS022177630;NSC-158340;CS-0317487;N-benzyloxycarbonyl-aminoacetaldehyde diethylacetal;N-benzyloxycarbonylaminoacetaldehyde diethyl acetal

Suppliers and Price of Benzyl 2,2-diethoxyethylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
Benzyl 2-
5mg
$ 496.00

Usbiological
Benzyl 2-
10mg
$ 496.00

Usbiological
Benzyl 2-
1mg
$ 496.00

Usbiological
Benzyl 2-
10mg
$ 496.00

Usbiological
Benzyl 2-
50mg
$ 460.00

Usbiological
Benzyl 2-
25mg
$ 460.00

Usbiological
Benzyl 2-
10mg
$ 446.00

Usbiological
Benzyl 2-
1mg
$ 446.00

Crysdot
Benzyl(2,2-diethoxyethyl)carbamate 97%
1g
$ 307.00

Biosynth Carbosynth
Benzyl 2,2-diethoxyethylcarbamate
500 mg
$ 250.00

Total 7 raw suppliers

Chemical Property of Benzyl 2,2-diethoxyethylcarbamate

Chemical Property:

Vapor Pressure:2.51E-06mmHg at 25°C
Boiling Point:391.2°C at 760 mmHg
Flash Point:190.4°C
PSA：56.79000
Density:1.083g/cm³
LogP:2.70280
XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:9
Exact Mass:267.14705815
Heavy Atom Count:19
Complexity:236

Purity/Quality:

99% ^*data from raw suppliers

Benzyl 2- ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(CNC(=O)OCC1=CC=CC=C1)OCC

Technology Process of Benzyl 2,2-diethoxyethylcarbamate

There total 3 articles about Benzyl 2,2-diethoxyethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 645-36-3
2,2-diethoxy-ethanamine

: 501-53-1,94274-21-2
benzyl chloroformate

: 60085-61-2
N-benzyloxycarbonylaminoacetaldehyde diethyl acetal

Guidance literature:: With triethylamine; In benzene; for 3h; Ambient temperature;
DOI:10.1248/cpb.28.2329

Reference yield:

: 113738-28-6
2-azidoethanal diethyl acetal

: 60085-61-2
N-benzyloxycarbonylaminoacetaldehyde diethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / tetrahydrofuran / 1 h / 0 °C

1.2: 20 °C

2.1: sodium carbonate / water / 2 h / 0 °C

With sodium carbonate; triphenylphosphine; In tetrahydrofuran; water;
DOI:10.1039/d0ob02018d

Reference yield:

: 621-62-5
chloroacetaldehyde diethyl acetal

: 60085-61-2
N-benzyloxycarbonylaminoacetaldehyde diethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium azide / dimethyl sulfoxide / 26 h / 130 °C

2.1: triphenylphosphine / tetrahydrofuran / 1 h / 0 °C

2.2: 20 °C

3.1: sodium carbonate / water / 2 h / 0 °C

With sodium azide; tetra-(n-butyl)ammonium iodide; sodium carbonate; triphenylphosphine; In tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1039/d0ob02018d