Technology Process of 4-PHENYL-[1,2,3]OXATHIAZINANE 2,2-DIOXIDE
There total 8 articles about 4-PHENYL-[1,2,3]OXATHIAZINANE 2,2-DIOXIDE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3-phenylpropyl sulfamate;
With
[Ru2(α,α,α′,α′-tetramethyl-1,3-benzenedipropionate)2]SbF6;
In
dichloromethane;
for 0.25h;
Molecular sieve;
With
bis(tert-butylcarbonyloxy)iodobenzene;
In
dichloromethane;
at 40 ℃;
for 24h;
chemoselective reaction;
DOI:10.1021/ja203576p
- Guidance literature:
-
With
silver hexafluoroantimonate; iron(III) phthalocyanine chloride; bis(tertbutylcarbonyloxy)iodobenzene;
In
toluene; acetonitrile;
at 20 ℃;
for 6h;
chemoselective reaction;
Inert atmosphere;
DOI:10.1021/ja211600g
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 76 percent / formic acid; chlorosulfonyl isocyanate / CH2Cl2; pyridine / 25 °C
2: 84 percent / MgO; PhI(OAc)2 / Rh2(oct)4 / CH2Cl2 / 40 °C
With
formic acid; isocyanate de chlorosulfonyle; [bis(acetoxy)iodo]benzene; magnesium oxide;
Rh2(Oct)4;
In
pyridine; dichloromethane;
DOI:10.1021/ja011033x
