2H-Tetrazol-5-amine,2-(1,1-dimethylethyl)-(9CI)

Base Information

• Chemical Name: 2H-Tetrazol-5-amine,2-(1,1-dimethylethyl)-(9CI)
• CAS No.: 59772-94-0
• Molecular Formula: C₅H₁₁N₅
• Molecular Weight: 141.176
• Mol file: 59772-94-0.mol

Synonyms:(2-tert-Butyl-2H-tetrazol-5-yl)amine;5-Amino-2-tert-butyltetrazole; NSC 282098

Chemical Property of 2H-Tetrazol-5-amine,2-(1,1-dimethylethyl)-(9CI)

Chemical Property:

• Vapor Pressure: 0.0055mmHg at 25°C
• Boiling Point: 274.1°C at 760 mmHg
• Flash Point: 119.6°C
• PSA: 69.62000
• Density: 1.29g/cm³
• LogP: 0.59150

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2H-Tetrazol-5-amine,2-(1,1-dimethylethyl)-(9CI)

There total 3 articles about 2H-Tetrazol-5-amine,2-(1,1-dimethylethyl)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

5-aminotetrazole (4418-61-5) + tert-butyl alcohol (75-65-0) → 2-tert-butyl-2H-tetrazol-5-amine (59772-94-0)

Guidance literature:

With sulfuric acid; for 0.666667h;

DOI:10.1007/BF00473965

Reference yield: 20.0%

5-aminotetrazole (4418-61-5) + tert-butyl alcohol (75-65-0) → 2-tert-butyl-2H-tetrazol-5-amine (59772-94-0) + 1-tert-butyl-5-aminotetrazole (59772-93-9) + 5-amino-1,3-di-tert-butyltetrazol-3-ium perchlorate

Guidance literature:

5-aminotetrazole; tert-butyl alcohol; With sulfuric acid; at 20 ℃; for 1h;

With sodium hydroxide; pH=4 - 5;

With perchloric acid; In water;

DOI:10.1134/S1070363210110228

Reference yield:

→ 2-tert-butyl-2H-tetrazol-5-amine (59772-94-0)

Guidance literature:

Tetrazol, t-Butanol, DCC, CuCl;

upstream raw materials:

5-aminotetrazole

tert-butyl alcohol

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