Acetic acid, [[3-butyl-3-ethyl-2,3,4,5-tetrahydro-7-(methylthio)-1,1-dioxido-5-phenyl-1 ,5-benzothiazepin-8-yl]oxy]-

Base Information

• Chemical Name: Acetic acid, [[3-butyl-3-ethyl-2,3,4,5-tetrahydro-7-(methylthio)-1,1-dioxido-5-phenyl-1 ,5-benzothiazepin-8-yl]oxy]-
• CAS No.: 358375-97-0
• Molecular Formula: C24H31NO5S2
• Molecular Weight: 477.646
• Mol file: 358375-97-0.mol

Synonyms:

Chemical Property of Acetic acid, [[3-butyl-3-ethyl-2,3,4,5-tetrahydro-7-(methylthio)-1,1-dioxido-5-phenyl-1 ,5-benzothiazepin-8-yl]oxy]-

Chemical Property:

Purity/Quality:

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Technology Process of Acetic acid, [[3-butyl-3-ethyl-2,3,4,5-tetrahydro-7-(methylthio)-1,1-dioxido-5-phenyl-1 ,5-benzothiazepin-8-yl]oxy]-

There total 1 articles about Acetic acid, [[3-butyl-3-ethyl-2,3,4,5-tetrahydro-7-(methylthio)-1,1-dioxido-5-phenyl-1 ,5-benzothiazepin-8-yl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-Dioxo-3-butyl-3-ethyl-5-phenyl-7-methylthio-8-ethoxycarbonylmethoxy-2,3,4,5-tetrahydro-1,5-benzothiazepine (358375-96-9) + 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran (96042-30-7) → 1,1-Dioxo-3-butyl-3-ethyl-5-phenyl-7-methylthio-8-carboxymethoxy-2,3,4,5-tetrahydro-1,5-benzothiazepine (358375-97-0)

Guidance literature:

With LiOH; acetic acid; In tetrahydrofuran; water;

Reference yield: 66.0%

4-(1-(R)-t-butoxycarbonyl-1-aminomethyl)phenol (501692-32-6) + 1,1-Dioxo-3-butyl-3-ethyl-5-phenyl-7-methylthio-8-carboxymethoxy-2,3,4,5-tetrahydro-1,5-benzothiazepine (358375-97-0) + HATU (200731-31-3,148893-10-1) → 1,1-Dioxo-3-butyl-3-ethyl-5-phenyl-7-methylthio-8-{N-[(R)-α-(t-butoxycarbonyl)-4hydroxybenzyl]carbamoylmethoxy}-2,3,4,5-tetrahydro-1,5-benzothiazepine

Guidance literature:

With 2,3-Lutidine; In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran;

Reference yield:

1,1-Dioxo-3-butyl-3-ethyl-5-phenyl-7-methylthio-8-carboxymethoxy-2,3,4,5-tetrahydro-1,5-benzothiazepine (358375-97-0) + methyl 3-amino-3-phenylpropanoate (14898-52-3) → 1,1-Dioxo-3-butyl-3-ethyl-5-phenyl-7-methylthio-8-[N-(α-methoxycarbonylmethyl-benzyl)carbamoylmethoxy]-2,3,4,5-tetrahydro-1,5-benzothiazepine (439089-08-4)

Guidance literature:

upstream raw materials:

1,1-Dioxo-3-butyl-3-ethyl-5-phenyl-7-methylthio-8-ethoxycarbonylmethoxy-2,3,4,5-tetrahydro-1,5-benzothiazepine

4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran

Downstream raw materials:

1,1-Dioxo-3-butyl-3-ethyl-5-phenyl-7-methylthio-8-[N-(α-methoxycarbonylmethyl-benzyl)carbamoylmethoxy]-2,3,4,5-tetrahydro-1,5-benzothiazepine

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