3-Isopropenyl-N,N-dimethylaniline

Base Information

Chemical Name:3-Isopropenyl-N,N-dimethylaniline
CAS No.:35843-88-0
Molecular Formula:C11H15N
Molecular Weight:161.247
Hs Code.:
DSSTox Substance ID:DTXSID60424086
Wikidata:Q82236521
Mol file:35843-88-0.mol

Synonyms:N,N-dimethyl-3-prop-1-en-2-ylaniline;3-ISOPROPENYL-N,N-DIMETHYLANILINE;35843-88-0;3-(CH3)2NC6H4C(CH3)=CH2;SCHEMBL610168;DTXSID60424086;AKOS006343064

Suppliers and Price of 3-Isopropenyl-N,N-dimethylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-ISOPROPENYL-N,N-DIMETHYLANILINE 95.00%
5MG
$ 500.97

Total 6 raw suppliers

Chemical Property of 3-Isopropenyl-N,N-dimethylaniline

Chemical Property:

Boiling Point:254.6±19.0 °C(Predicted)
PKA:4.83±0.10(Predicted)
PSA：3.24000
Density:0.930±0.06 g/cm3(Predicted)
LogP:2.78570
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:161.120449483
Heavy Atom Count:12
Complexity:160

Purity/Quality:

99.0% ^*data from raw suppliers

3-ISOPROPENYL-N,N-DIMETHYLANILINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=C)C1=CC(=CC=C1)N(C)C

Technology Process of 3-Isopropenyl-N,N-dimethylaniline

There total 5 articles about 3-Isopropenyl-N,N-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 16518-62-0
3-bromo-N,N-dimethylaniline

: 126726-62-3
2-isopropenyl-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 35843-88-0
2-<3-(Dimethylamino)phenyl>propene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; toluene; at 85 ℃; for 7h;

Reference yield: 72.0%

: 92546-72-0
2-(3-(dimethylamino)phenyl)propan-2-ol

: 35843-88-0
2-<3-(Dimethylamino)phenyl>propene

Guidance literature:: With potassium hydrogensulfate; In 5,5-dimethyl-1,3-cyclohexadiene; at 150 ℃; for 1h;
DOI:10.1021/jo500140y

Reference yield:

: 16518-62-0
3-bromo-N,N-dimethylaniline

: 35843-88-0
2-<3-(Dimethylamino)phenyl>propene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; cyclohexane / 0.25 h / -78 °C / Schlenk technique; Inert atmosphere

1.2: 0.25 h / -78 °C / Schlenk technique; Inert atmosphere

2.1: potassium hydrogensulfate / 5,5-dimethyl-1,3-cyclohexadiene / 1 h / 150 °C

With potassium hydrogensulfate; n-butyllithium; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; cyclohexane;
DOI:10.1021/jo500140y