Fluoranthene-3-boronic acid

Base Information

• Chemical Name: Fluoranthene-3-boronic acid
• CAS No.: 359012-63-8
• Molecular Formula: C16H11BO2
• Molecular Weight: 246.073
• Hs Code.: 2931900090
• Mol file: 359012-63-8.mol

Synonyms:fluoranthen-3-ylboronic acid;

Chemical Property of Fluoranthene-3-boronic acid

Chemical Property:

• Boiling Point: 509.4±33.0 °C(Predicted)
• PKA: 8.53±0.30(Predicted)
• PSA: 40.46000
• Density: 1.35±0.1 g/cm3(Predicted)
• LogP: 2.16700
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C
• Water Solubility.: Slightly soluble in water.

Purity/Quality:

98% ^*data from raw suppliers

Fluoranthene-3-boronic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Description: Fluoranthene-3-boronic acid can be used in the production of optics (it is a useful OLEDs material), and can also be applied in novel molecular architectures and functional materials.
• Uses: Fluoranthene-3-boronic acid is used in the production of optics. It is also applied in novel molecular architectures and functional materials. Stable under recommended storage conditions. Store away from oxidizing agents.

Technology Process of Fluoranthene-3-boronic acid

There total 3 articles about Fluoranthene-3-boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Triisopropyl borate (5419-55-6) + 3-bromofluoranthene (13438-50-1) → 7,12-diphenylbenzo[k]fluoranthene-3-boronic acid (359012-63-8)

Guidance literature:

With n-butyllithium; water; In tetrahydrofuran; at -80 ℃; for 0.25h;

Reference yield: 65.0%

3-bromofluoranthene (13438-50-1) → 7,12-diphenylbenzo[k]fluoranthene-3-boronic acid (359012-63-8)

Guidance literature:

3-bromofluoranthene; With n-butyllithium; In tetrahydrofuran; hexane; for 1h;

With Trimethyl borate; In tetrahydrofuran; hexane;

With water; ammonium chloride; In tetrahydrofuran; hexane;

Reference yield:

fluoranthene (206-44-0) → 7,12-diphenylbenzo[k]fluoranthene-3-boronic acid (359012-63-8)

Guidance literature:

Multi-step reaction with 2 steps

1: bromine / nitrobenzene / 20 h / 20 °C

2: n-butyllithium / hexane; tetrahydrofuran / 1 h

With n-butyllithium; bromine; In tetrahydrofuran; hexane; nitrobenzene;

upstream raw materials:

3-bromofluoranthene

fluoranthene

Triisopropyl borate

Downstream raw materials:

3-(4-bromophenyl)fluoranthene

C₃₅H₂₂N₂

4-(fluoranthen-3-yl)phenylboronic acid

C₂₈H₁₇Br

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