1,3-Dichloro-1,1,1,3,3,3-hexaphenyl-1lambda~5~,3lambda~5~-dibismoxane

Base Information

Chemical Name:1,3-Dichloro-1,1,1,3,3,3-hexaphenyl-1lambda~5~,3lambda~5~-dibismoxane
CAS No.:35952-85-3
Molecular Formula:C₃₆H₃₀Bi₂Cl₂O
Molecular Weight:967.5
Hs Code.:
DSSTox Substance ID:DTXSID30587011
Wikidata:Q82479244
Mol file:35952-85-3.mol

Synonyms:35952-85-3;DTXSID30587011;1,3-Dichloro-1,1,1,3,3,3-hexaphenyl-1lambda~5~,3lambda~5~-dibismoxane

Suppliers and Price of 1,3-Dichloro-1,1,1,3,3,3-hexaphenyl-1lambda~5~,3lambda~5~-dibismoxane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Dichloro-1,1,1,3,3,3-hexaphenyl-1lambda~5~,3lambda~5~-dibismoxane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:8
Exact Mass:966.12817
Heavy Atom Count:41
Complexity:664

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)[Bi](C2=CC=CC=C2)(C3=CC=CC=C3)(O[Bi](C4=CC=CC=C4)(C5=CC=CC=C5)(C6=CC=CC=C6)Cl)Cl

Technology Process of 1,3-Dichloro-1,1,1,3,3,3-hexaphenyl-1lambda~5~,3lambda~5~-dibismoxane

There total 4 articles about 1,3-Dichloro-1,1,1,3,3,3-hexaphenyl-1lambda~5~,3lambda~5~-dibismoxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 119987-71-2
μ-oxobis[(4-methylbenzenesulfonato)triphenylbismuth]

: 7647-14-5
sodium chloride

: 35952-85-3
μ-oxo-bis(triphenylbismuth chloride)

Guidance literature:: In water; acetone; byproducts: sodium 4-methylbenzenesulfonate; a soln. of NaCl in H2O added to a soln. of Bi compd. in acetone; crystals washed (H2O), dried;
DOI:10.1007/s11176-005-0011-x

Reference yield:

: 507233-69-4,594-30-9,28719-54-2
triphenyl bismuth ⁽²⁺⁾; dichloride

: 35952-85-3
μ-oxo-bis(triphenylbismuth chloride)

Guidance literature:: With NaOH; In methanol; acetone; (C6H5)3BiCl2 in acetone mixed with NaOH in methanol in equiv.amt. 2 h at 20°C;filtration,graduated by boiling in vac., added H2O; crystn. from CHCl3-petroleum ether;
DOI:10.1016/S0022-328X(00)80680-4