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7647-14-5 Usage

Definition

ChEBI: An inorganic chloride salt having sodium(1+) as the counterion.

Brand name

Broncho Saline (Blairex).

Air & Water Reactions

Water soluble.

Purification Methods

It is recrystallised from a saturated aqueous solution (2.7mL/g) by passing in HCl gas, or by adding EtOH or acetone. It can be freed from bromide and iodide impurities by adding chlorine water to an aqueous solution and boiling it for some time to expel free bromine and iodine. Traces of iron can be removed by prolonged boiling of solid NaCl in 6M HCl; the crystals are then washed with EtOH and dried at ca 100o. Sodium chloride has been purified by sublimation in a stream of pre-purified N2 and collected by electrostatic discharge [Ross & Winkler J Am Chem Soc 76 2637 1954]. For use as a primary analytical standard, analytical reagent grade NaCl should be finely ground, dried in an electric furnace at 500-600o in a platinum crucible, and allowed to cool in a desiccator. For most purposes, however, drying at 110-120o is satisfactory.

Chemical Properties

Sodium chloride, NaCl, also known as common salt and halite, is a white crystalline solid.It is soluble in water,slightly soluble in alcohol, and melts at 804 °C (1480 °F). Sodium chloride is the most important sodium mineral and occurs naturally in seawater, underground deposits, and brine wells.Sodiumchlorideis a basic raw material for the production of chlorine,sodium hypochlorite, sodium bisulfate,soda ash, and hydrogen chloride. Sodium chloride is also used in food preparation, fertilizers, and by highway departments to control icy road conditions.

Preparation

Sodium chloride is produced by solar evaporation of seawater or brine from underground salt deposits. It also is produced by mining rock salt. The commercial product contains small amounts of calcium and magnesium chlorides.

Fire Hazard

Literature sources indicate that Sodium chloride is nonflammable.

Description

Sodium chloride is widely distributed in nature. Oceans are the vast source of sodium chloride. It occurs in seawater at an average concentration of 2.68 wt%. It also occurs in many inland saline waters and in salt deposits in sedimentary rocks, as the mineral halite.
Sodium chloride is probably the most important salt of both sodium and chlorine. Sodium chloride, common table salt, is an essential component of most food preparation, imparting flavor to food and providing the sodium nutritional requirement. Also, it is used for preserving food. Therapeutically, NaCl solution is used to combat dehydration as an electrolyte replenisher, and it is an emetic.
The most important applications of sodium chloride in the chemical industry are in making a number of important industrial chemicals such as hydrochloric acid, sodium hydroxide, sodium carbonate, and metallic sodium. It is the starting material in manufacturing these substances. Other uses are in dyeing and printing fabrics, glazing pottery, in making soap, and for curing hides. Sodium chloride is a component of many freezing mixtures.

Uses

Natural salt is the source of chlorine and of sodium as well as of all, or practically all, their Compounds, e.g., hydrochloric acid, chlorates, sodium carbonate, hydroxide, etc.; for preserving foods; manufacture of soap, to salt out dyes; in freezing mixtures; for dyeing and printing fabrics, glazing pottery, curing hides; metallurgy of tin and other metals.

Reactivity Profile

Sodium chloride is generally unreactive. Releases gaseous hydrogen chloride if mixed with a concentrated nonvolatile acid such as sulfuric acid.

Uses

Used as an electrolyte; buffers ; matrix modification.

General Description

A white crystalline solid. Commercial grade usually contains some chlorides of calcium and magnesium which absorb moisture and cause caking.

Uses

Used in biochemistry and molecular biology applications; a component of PBS and SSC buffers

Uses

Facilitates the cross-coupling of organostannanes with iodides without using palladium.1
InChI:InChI=1/ClH.Na/h1H;/q;+1/p-1/i;1-1

7647-14-5 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Sigma-Aldrich (NIST975A)  Isotopic standard for chlorine  NIST SRM 975a 7647-14-5 NIST975A 10,786.23CNY Detail
USP (1613804)  Sodiumchloride  United States Pharmacopeia (USP) Reference Standard 7647-14-5 1613804-1G 4,662.45CNY Detail
Sigma-Aldrich (S0817)  Sodiumchloridesolution  0.85% 7647-14-5 S0817-5GA 902.07CNY Detail
Sigma-Aldrich (S0817)  Sodiumchloridesolution  0.85% 7647-14-5 S0817-1GA 324.09CNY Detail
Sigma (59222C)  Sodiumchloridesolution  5 M 7647-14-5 59222C-1000ML 560.43CNY Detail
Sigma (59222C)  Sodiumchloridesolution  5 M 7647-14-5 59222C-500ML 324.09CNY Detail
Sigma-Aldrich (S6546)  Sodiumchloridesolution  5 M 7647-14-5 S6546-4L 1,804.14CNY Detail
Sigma-Aldrich (S6546)  Sodiumchloridesolution  5 M 7647-14-5 S6546-1L 541.71CNY Detail
Sigma-Aldrich (S9625)  Sodiumchloride  ReagentPlus®, ≥99% 7647-14-5 S9625-10KG 2,008.89CNY Detail
Sigma-Aldrich (S9625)  Sodiumchloride  ReagentPlus®, ≥99% 7647-14-5 S9625-5KG 1,891.89CNY Detail
Sigma-Aldrich (S9625)  Sodiumchloride  ReagentPlus®, ≥99% 7647-14-5 S9625-1KG 628.29CNY Detail
Sigma-Aldrich (S9625)  Sodiumchloride  ReagentPlus®, ≥99% 7647-14-5 S9625-500G 445.77CNY Detail

7647-14-5SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 16, 2017

Revision Date: Aug 16, 2017

1.Identification

1.1 GHS Product identifier

Product name sodium chloride

1.2 Other means of identification

Product number -
Other names sodium hydrochloride

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:7647-14-5 SDS

7647-14-5Synthetic route

Iodine monochloride
7790-99-0

Iodine monochloride

sodium sulfate
7757-82-6

sodium sulfate

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
evaporated, with excess of ICl;100%
evaporated, with excess of ICl;100%
sodium nitrate
7631-99-4

sodium nitrate

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
With hydrogenchloride In neat (no solvent) passing dry HCl over NaNO3 at 130°C over period of 2 to 3 h;; slow heating to 400°C to get rid of HNO3 traces;;100%
With HCl In neat (no solvent) passing dry HCl over NaNO3 at 130°C over period of 2 to 3 h;; slow heating to 400°C to get rid of HNO3 traces;;100%
dihydrogen peroxide
7722-84-1

dihydrogen peroxide

chlorine
7782-50-5

chlorine

sodium hydroxide
1310-73-2

sodium hydroxide

oxygen
7782-44-7

oxygen

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In water H2O2 soln. poured onto porous glass plate within the singlet O2 generator (closed glass system, under Ar), spent liquid discarded into the lower flask, Cl2 (1-2 kPa) admitted, alkali soln. poured in, evolution of singlet O2 over a period of 12-16 min.; luminiscence spectroscopy, calorimetry;A 100%
B n/a
dineopentylgalliumchloride
113976-09-3

dineopentylgalliumchloride

ammonia
7664-41-7

ammonia

A

((CH3)3CCH2)2GaNH2

((CH3)3CCH2)2GaNH2

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
With sodium In neat (no solvent) Ar-atmosphere; stirring (-70°C, 1 h); evapn., extg. (pentane); elem. anal.;A n/a
B 100%
sodium tetrahydroborate
16940-66-2

sodium tetrahydroborate

lithium chloride

lithium chloride

A

lithium borohydride

lithium borohydride

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
With 1,3-dioxolane In further solvent(s) (N2); salts mixt. (1/1 molar ratio) stirred at 25-74°C for 1-48 h in 1,3-dioxolane; heated (vac.);A 99%
B n/a
With isopropylamine In further solvent(s) (N2); salts mixt. (1/1 molar ratio) stirred at 25-34°C for 2-8 hin isopropylamine; heated (vac.);A 97-100
B n/a
With C4H8O In tetrahydrofuran (N2); salts mixt. (1/1 molar ratio) stirred at 25-67°C for 1-48 h in THF; heated (vac.);
With diethyl ether In diethyl ether (N2); salts mixt. (1/1 molar ratio) stirred at 35°C for 1-48 h in Et2O; heated (vac.);
With 1,2-dimethoxyethane In 1,2-dimethoxyethane (N2); salts mixt. (1/1 molar ratio) stirred at 0-85°C for 1-72 hin monoglyme; heated (vac.);
hydrogenchloride
7647-01-0

hydrogenchloride

sodium carbonate
497-19-8

sodium carbonate

A

H2CO3*CH3CH2OCH2CH3
116973-99-0

H2CO3*CH3CH2OCH2CH3

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In diethyl etherA 99%
B n/a
In diethyl etherA 99%
B n/a
hydrogenchloride
7647-01-0

hydrogenchloride

sodium carbonate
497-19-8

sodium carbonate

A

Kohlenstoffoxid-bis-(hydroxid)-mono-dimethylaetherat
3890-73-1

Kohlenstoffoxid-bis-(hydroxid)-mono-dimethylaetherat

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In Dimethyl etherA 99%
B n/a
In Dimethyl etherA 99%
B n/a
Na2[(C10H8)(Ga(CH2C(CH3)3)2Cl)2]

Na2[(C10H8)(Ga(CH2C(CH3)3)2Cl)2]

ammonia
7664-41-7

ammonia

A

((CH3)3CCH2)2GaNH2

((CH3)3CCH2)2GaNH2

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In tetrahydrofuran Ar-atmosphere; stirring (-78°C, 18 h); evapn. (vac.), drying (dynamic vac., 40 h), extg. (pentane), filtering, subliming (55°C);A 52%
B 99%
sodium azide

sodium azide

copper dichloride

copper dichloride

A

copper(I) nitride

copper(I) nitride

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In tetrahydrofuran byproducts: N2; High Pressure; CuCl2 and NaN3 ground, placed into a stainless steel reactor, solvent added, sealed, heated to ca. 50°C, ca. 100°C, and 185°C with regulated rates (the total react. time of ca. 3-5 d); cooled to room temp., dried (vac.), NaCl sepd. with MeOH under N2, filtered, dried (vac.); obtained as nanocrystals;A 98%
B n/a
In toluene byproducts: N2; High Pressure; CuCl2 and NaN3 ground, placed into a stainless steel reactor, solvent added, sealed, heated to ca. 50°C, ca. 100°C, and 185°C with regulated rates (the total react. time of ca. 3-5 d); cooled to room temp., dried (vac.), NaCl sepd. with MeOH under N2, filtered, dried (vac.); obtained as nanocrystals;A 85%
B n/a
In m-xylene at 116-135°C for 14 h to 1.5 d; not isolated, detected by IR, XRD;
(naphthalene)Yb2(THF)3(NaCl)3

(naphthalene)Yb2(THF)3(NaCl)3

A

ytterbium(III) oxide

ytterbium(III) oxide

B

naphthalene
91-20-3

naphthalene

C

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
With air In tetrahydrofuran stirred for 18 h under dry air; centrifuged, washed with benzene and water (Yb2O3), naphthalene detd. by GLC in the organic layer, aq. soln. contains NaCl;A 98%
B 98%
C 96%
(vinyl)trimethoxylsilane
2768-02-7

(vinyl)trimethoxylsilane

sodium
7440-23-5

sodium

copper dichloride

copper dichloride

butan-1-ol
71-36-3

butan-1-ol

A

copper sodium vinylsiloxane

copper sodium vinylsiloxane

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In methanol; water Na addn. to methanolic soln. of Si-compd., refluxing (1 h), methanolic soln. of Cu-compd. addn., refluxing (2 h), MeOH distillation off with simultaneous addn. of butanol, refluxing (15 min); NaCl filtration off, solvent evapn. to crystn., after 48 h crystals sepn., drying (20°C); elem. anal.;A 97.6%
B 98%
ethanol
64-17-5

ethanol

3-(trimethoxysilyl)propan-1-amine
13822-56-5

3-(trimethoxysilyl)propan-1-amine

sodium hydroxide
1310-73-2

sodium hydroxide

copper dichloride

copper dichloride

A

copper sodium γ-aminopropylsiloxane

copper sodium γ-aminopropylsiloxane

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In methanol; water Si-compd. dissoln. in MeOH, aq. soln. of NaOH addn., refluxing (1 h), soln. of Cu-compd. in MeOH addn., refluxing (30 min), MeOH distillation off with simultaneous addn. of EtOH; NaCl filtration off, solvent removing; elem. anal.;A 93%
B 98%
2,2,4,4,6,6-hexamethyl-1,3,5,2,4,6-trithiatristanninane
16892-64-1

2,2,4,4,6,6-hexamethyl-1,3,5,2,4,6-trithiatristanninane

N-chloro-p-chlorobenzenesulfonamide sodium salt
30066-82-1

N-chloro-p-chlorobenzenesulfonamide sodium salt

A

CH3OSn(CH3)2S(NSO2C6H4Cl)Sn(CH3)2SSn(CH3)2NHSO2C6H4Cl
206008-10-8

CH3OSn(CH3)2S(NSO2C6H4Cl)Sn(CH3)2SSn(CH3)2NHSO2C6H4Cl

B

sulfur
7704-34-9

sulfur

C

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In methanol soln. of N-compd. addn. to soln. of Sn compd. (vacuum, stirring), heating (50°C, 30 min); mixture cooling (ice bath), ppt. filtration off and extracting with water to remove NaCl and with acetone to remove S, alcoholic filtrate vacuumevapn., residue treating with diethyl ether, soln. decanting and vacuum evapn.; elem. anal.;A 92%
B 33%
C 98%
phenyl trimethylsiloxane
2996-92-1

phenyl trimethylsiloxane

sodium
7440-23-5

sodium

copper dichloride

copper dichloride

A

copper sodium phenylsiloxane

copper sodium phenylsiloxane

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In ethanol; water elem. anal.;A 90.3%
B 96%
(vinyl)trimethoxylsilane
2768-02-7

(vinyl)trimethoxylsilane

sodium hydroxide
1310-73-2

sodium hydroxide

manganese(ll) chloride

manganese(ll) chloride

butan-1-ol
71-36-3

butan-1-ol

A

manganese vinylsiloxane

manganese vinylsiloxane

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In methanol; water soln. of NaOH addn. to soln. of Si-compd., refluxing, soln. of Mn-compd.addn., refluxing, MeOH distillation off with simultaneous addn. of buta nol; NaCl filtration off, solvent evapn.; elem. anal.;A 87%
B 95.5%
tributyltin chloride
1461-22-9

tributyltin chloride

sodium
7440-23-5

sodium

benzildioxime
23873-81-6

benzildioxime

A

C6H5C(NOH)C(NO)C6H5Sn(CH2CH2CH2CH3)3
256524-18-2

C6H5C(NOH)C(NO)C6H5Sn(CH2CH2CH2CH3)3

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In isopropyl alcohol; benzene strictly anhydrous conditions; addn. of Na to excess of i-PrOH, refluxing (0.5 h), cooling, addn. of oxime, refluxing (2 h), cooling, addn. of stoichiom. amt. of Sn compound in benzene, refluxing (2 h); sovent removal (reduced pressure), filtration off of NaCl, crystn. (benzene/petroleum ether); elem. anal.;A 95%
B n/a
CYANAMID
420-04-2

CYANAMID

cyanogen chloride
506-77-4

cyanogen chloride

A

sodium N-cyanoisourea
76989-89-4

sodium N-cyanoisourea

B

sodium dicyanamide
1934-75-4

sodium dicyanamide

C

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
With sodium hydroxide In water at 70 - 75℃; under 1050.11 Torr; pH=7.2 - 8.0; Purification / work up;A n/a
B 94%
C n/a
sodium tetrahydroborate
16940-66-2

sodium tetrahydroborate

aluminium trichloride
7446-70-0

aluminium trichloride

BF3-triglymate

BF3-triglymate

A

aluminum(III) fluoride
7784-18-1

aluminum(III) fluoride

B

sodium chloride
7647-14-5

sodium chloride

C

diborane
19287-45-7

diborane

Conditions
ConditionsYield
In further solvent(s) soln. NaBH4 in triglyme was added slowly for 2-3 h at room temp. to BF3-triglyme, AlCl3 in triglyme; B2H6 was absorbed with THF;A n/a
B n/a
C 94%
sodium tetrahydroborate
16940-66-2

sodium tetrahydroborate

aluminium trichloride
7446-70-0

aluminium trichloride

BF3-tetraglymate

BF3-tetraglymate

A

aluminum(III) fluoride
7784-18-1

aluminum(III) fluoride

B

sodium chloride
7647-14-5

sodium chloride

C

diborane
19287-45-7

diborane

Conditions
ConditionsYield
In further solvent(s) soln. NaBH4 in triglyme was added slowly for 2-3 h at room temp. to BF3-tetraglyme, AlCl3 in triglyme; B2H6 was absorbed with THF;A n/a
B n/a
C 94%
indium(III) chloride
10025-82-8

indium(III) chloride

sodium pentamethylcyclopentadienide

sodium pentamethylcyclopentadienide

A

indiumpentamethylcyclopentadienide

indiumpentamethylcyclopentadienide

B

decamethylfulvalene
69446-48-6

decamethylfulvalene

C

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In tetrahydrofuran soln. of InCl3 and Na-compd. mixed,, stirred for 18h; molar ratio In-compd : Li-compd = 1:3; exclusion of air and moisture; solvent removed, pentane distilled onto poducts, sublimation; elem. anal.;A 65.9%
B 83.9%
C 94%
CH3C6H4NCHC6H2(CH3)(CO)OHRh(P(C6H5)3)2Cl2

CH3C6H4NCHC6H2(CH3)(CO)OHRh(P(C6H5)3)2Cl2

sodium nitrite
7632-00-0

sodium nitrite

CH(O)C6H2(CH3)(CO)ORh(P(C6H5)3)2NO2
222532-71-0

CH(O)C6H2(CH3)(CO)ORh(P(C6H5)3)2NO2

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
With H2O In dichloromethane; acetone byproducts: CH3C6H4NH2*HCl; stirring (0.5 h), evapn. (reduced pressure); filtering, washing (H2O), drying (vac.); elem. anal.;A 94%
B n/a
phenyl trimethylsiloxane
2996-92-1

phenyl trimethylsiloxane

sodium
7440-23-5

sodium

manganese(ll) chloride

manganese(ll) chloride

butan-1-ol
71-36-3

butan-1-ol

A

manganese phenylsiloxane

manganese phenylsiloxane

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In methanol; ethanol elem. anal.;A 42.5%
B 94%
sodium tetrafluoroborate
13755-29-8

sodium tetrafluoroborate

trans-bis(triphenylphosphine)palladium dichloride
28966-81-6

trans-bis(triphenylphosphine)palladium dichloride

p-methoxyphenylisocyanide
10349-38-9

p-methoxyphenylisocyanide

trans-{(PPh3)2Pd(CNC6H4-p-OMe)Cl}BF4
110313-86-5

trans-{(PPh3)2Pd(CNC6H4-p-OMe)Cl}BF4

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In acetone under inert gas; dropwise addn. of the isocyanide in acetone to the suspn. of the Pd complex in acetone in presence of NaBF4 at room temp.; stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtered and concd., addn. of Et2O yields the solid; elem. anal.;A 93%
B n/a
sodium tetrafluoroborate
13755-29-8

sodium tetrafluoroborate

trans-dichlorobis(triphenylphosphine)platinum(II)
14056-88-3

trans-dichlorobis(triphenylphosphine)platinum(II)

Cyclohexyl isocyanide
931-53-3

Cyclohexyl isocyanide

trans-{(PPh3)2Pt(CNC6H11)Cl}BF4
110313-80-9

trans-{(PPh3)2Pt(CNC6H11)Cl}BF4

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In acetone under inert gas; dropwise addn. of the isocyanide in acetone to the suspn. of the Pt complex in acetone in presence of NaBF4 at room temp.; stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtered and concd., addn. of Et2O yields the solid; elem. anal.;A 92%
B n/a
hydrogenchloride
7647-01-0

hydrogenchloride

sodium hydrogen sulfide

sodium hydrogen sulfide

A

hydrogen sulfide
7783-06-4

hydrogen sulfide

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
-78°C;A n/a
B 92%
picoline
108-89-4

picoline

indium(III) chloride
10025-82-8

indium(III) chloride

sodium 3,5-di-tert-butyl-o-benzosemiquinolate
4679-12-3, 61373-02-2

sodium 3,5-di-tert-butyl-o-benzosemiquinolate

A

[InCl(((CH3)3C)2C6H2O2)(CH3C5H4N)2]
159650-04-1

[InCl(((CH3)3C)2C6H2O2)(CH3C5H4N)2]

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In tetrahydrofuran byproducts: H2; N2, blue soln. of semiquinone sodium salt added dropwise over 1 h to a soln. of In-salt, stirred for 2 h at room temp., NaCl removed from intermediate products by filtrn., excess 4-picoline added to the filtrate; collected, dried, recrystd. (toluene/THF); elem. anal.; formn. of In(I)and other species also discussed;A 50%
B 92%
sodium azide

sodium azide

chlorobis[3-(dimethylamino)propyl]aluminium
199918-52-0

chlorobis[3-(dimethylamino)propyl]aluminium

azidobis[3-(dimethylamino)propyl]aluminium
185536-86-1

azidobis[3-(dimethylamino)propyl]aluminium

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In tetrahydrofuran N2-atmosphere; refluxing (15 h); evapn. (vac.), sublimation (100°C, 10E-04 Torr);A 92%
B n/a
sodium
7440-23-5

sodium

acetyl chloride
75-36-5

acetyl chloride

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
With diethyl malonate In ethanol; toluene Na was dissolved in EtOH at room temp., diethylmalonate was added, toluene was added, soln. phenacyl chloride in toluene was added at room temp.; ppt. was centrifugated and washed with EtOH; powder X-ray diffraction;92%
sodium dicarbonyl(cyclopentadienyl)ferrate

sodium dicarbonyl(cyclopentadienyl)ferrate

1-chloro-2-chloromethyl-1,1,2,2-tetramethyl-disilane
18143-50-5

1-chloro-2-chloromethyl-1,1,2,2-tetramethyl-disilane

A

(η5-C5H5)Fe(CO)2SiMe2SiMe2CH2Fe(CO)2(η5-C5H5)
255852-10-9

(η5-C5H5)Fe(CO)2SiMe2SiMe2CH2Fe(CO)2(η5-C5H5)

B

sodium chloride
7647-14-5

sodium chloride

Conditions
ConditionsYield
In tetrahydrofuran to THF soln. (Fp)Na was added to THF soln. ClCH2SiMe2SiMe2Cl at ambienttemp. and stirred for 2 h; solvent was removed and product was extd. into hexane, solvent was evapd. and residue was chromed. on silica using hexane as eluent; elem. anal.;A 91%
B n/a
sodium tetrahydroborate
16940-66-2

sodium tetrahydroborate

sodium tetrafluoroborate
13755-29-8

sodium tetrafluoroborate

aluminium trichloride
7446-70-0

aluminium trichloride

A

aluminum(III) fluoride
7784-18-1

aluminum(III) fluoride

B

sodium chloride
7647-14-5

sodium chloride

C

diborane
19287-45-7

diborane

Conditions
ConditionsYield
In further solvent(s) soln. NaBH4 in triglyme (tetraglyme) was added slowly for 2-3 h at roomtemp. to NaBF4 and AlCl3 in triglyme (tetraglyme); B2H6 was absorbed with THF;A n/a
B n/a
C 90%
ammonium carbonate

ammonium carbonate

ammonia
7664-41-7

ammonia

sodium chloride
7647-14-5

sodium chloride

sodium carbonate
497-19-8

sodium carbonate

Conditions
ConditionsYield
In water NH3 passed into a soln. of (NH4)2CO3-NaCl until satn.; product free of Cl and NH3;100%
In water NH3 passed into a soln. of (NH4)2CO3-NaCl until satn.; product free of Cl and NH3;100%
zirconium
7440-67-7

zirconium

beryllium

beryllium

zirconium(IV) chloride
10026-11-6

zirconium(IV) chloride

sodium chloride
7647-14-5

sodium chloride

Na4[(Zr6Be)Cl16]

Na4[(Zr6Be)Cl16]

Conditions
ConditionsYield
In neat (no solvent) stoichiometric mixture, sealed Ta container, 800-850°C;100%
In neat (no solvent) heating of stoich. amts. of reagents in a sealed Ta tube at 700-860°C for 2-3 weeks; identified by single crystal X-ray diffraction;>90
In neat (no solvent) mixt. of Zr, ZrCl4, NaCl and Be was sealed under Ar in Nb or Ta ampule; heated;
fluorosilicic acid

fluorosilicic acid

sodium chloride
7647-14-5

sodium chloride

sodium hexafluorosilicate

sodium hexafluorosilicate

Conditions
ConditionsYield
In water pptn. from H2SiF6 soln. (12%) by NaCl soln. (60% excess);;100%
In water pptn. from H2SiF6 soln. (12%) by NaCl soln. (60% excess);;100%
In water pptn. from H2SiF6 soln. (12%) by NaCl soln. (20% excess);;90%
sodium chlorate

sodium chlorate

uranium oxide

uranium oxide

sodium chloride
7647-14-5

sodium chloride

sodium uranate

sodium uranate

Conditions
ConditionsYield
In neat (no solvent) gradual addn. of NaClO3 to melt of U3O8 and NaCl; very slow, but complete react.;;100%
In neat (no solvent) gradual addn. of NaClO3 to melt of U3O8 and NaCl; very slow, but complete react.;;100%
uranium oxide

uranium oxide

sodium carbonate
497-19-8

sodium carbonate

sodium chloride
7647-14-5

sodium chloride

sodium uranate

sodium uranate

Conditions
ConditionsYield
In neat (no solvent) using same amt. of NaCl and Na2CO3;;100%
In neat (no solvent) using same amt. of NaCl and Na2CO3;;100%
chlorine
7782-50-5

chlorine

sodium chloride
7647-14-5

sodium chloride

sodium chlorate

sodium chlorate

Conditions
ConditionsYield
In water at 353 K, in diaphragm electrolyzer, at pH 2.1-3.0;100%
In water byproducts: NaOCl; at 353 K, in diaphragm electrolyzer, at pH 4.0-6.0;98.1%
In water byproducts: NaOCl; at 353 K, in diaphragm electrolyzer, at pH 6.0-8.0;96%
m-carboran-9-yl(phenyl)iodonium tetrafluoroborate
81353-33-5

m-carboran-9-yl(phenyl)iodonium tetrafluoroborate

sodium chloride
7647-14-5

sodium chloride

A

iodobenzene
591-50-4

iodobenzene

B

9-chloro-m-carborane
17819-85-1

9-chloro-m-carborane

Conditions
ConditionsYield
In chloroform; water mixt. of aryl(m-carboran-9-yl)iodonium tetrafluoroborate, NaF, water and chloroform was vigorously stirred under reflux at 56°C, 1 h; internal standard (chlorobenzene) added and org. layer was analysed by GLC;A 100%
B 100%
4-methoxyphenyl(m-carboran-9-yl)iodonium tetrafluoroborate
99506-45-3

4-methoxyphenyl(m-carboran-9-yl)iodonium tetrafluoroborate

sodium chloride
7647-14-5

sodium chloride

A

9-iodo-m-carborane
17157-02-7

9-iodo-m-carborane

B

9-chloro-m-carborane
17819-85-1

9-chloro-m-carborane

C

para-iodoanisole
696-62-8

para-iodoanisole

D

methoxybenzene
100-66-3

methoxybenzene

Conditions
ConditionsYield
In chloroform; water mixt. of aryl(m-carboran-9-yl)iodonium tetrafluoroborate, NaCl, water and chloroform was vigorously stirred under reflux at 56°C, 2-2.5 h; internal standard (chlorobenzene) added and org. layer was analysed by GLC;A 0%
B 100%
C 100%
D 0%
4-fluorophenyl(m-carboran-9-yl)iodonium tetrafluoroborate
99506-39-5

4-fluorophenyl(m-carboran-9-yl)iodonium tetrafluoroborate

sodium chloride
7647-14-5

sodium chloride

A

fluorobenzene
462-06-6

fluorobenzene

B

9-iodo-m-carborane
17157-02-7

9-iodo-m-carborane

C

9-chloro-m-carborane
17819-85-1

9-chloro-m-carborane

D

4-fluoro-1-iodobenzene
352-34-1

4-fluoro-1-iodobenzene

Conditions
ConditionsYield
In chloroform; water mixt. of aryl(m-carboran-9-yl)iodonium tetrafluoroborate, NaCl, water and chloroform was vigorously stirred under reflux at 56°C, 2-2.5 h; internal standard (chlorobenzene) added and org. layer was analysed by GLC;A 0%
B 0%
C 100%
D 100%
3-nitrophenyl(m-carboran-9-yl)iodonium tetrafluoroborate
99506-41-9

3-nitrophenyl(m-carboran-9-yl)iodonium tetrafluoroborate

sodium chloride
7647-14-5

sodium chloride

A

m-iodonitrobenzene
645-00-1

m-iodonitrobenzene

B

9-iodo-m-carborane
17157-02-7

9-iodo-m-carborane

C

9-chloro-m-carborane
17819-85-1

9-chloro-m-carborane

D

nitrobenzene
98-95-3

nitrobenzene

Conditions
ConditionsYield
In chloroform; water mixt. of aryl(m-carboran-9-yl)iodonium tetrafluoroborate, NaCl, water and chloroform was vigorously stirred under reflux at 56°C, 2-2.5 h; internal standard (chlorobenzene) added and org. layer was analysed by GLC;A 100%
B 0%
C 100%
D 0%
2,4,6-trimethylphenyl(m-carboran-9-yl)iodonium tetrafluoroborate
99506-43-1

2,4,6-trimethylphenyl(m-carboran-9-yl)iodonium tetrafluoroborate

sodium chloride
7647-14-5

sodium chloride

A

9-iodo-m-carborane
17157-02-7

9-iodo-m-carborane

B

9-chloro-m-carborane
17819-85-1

9-chloro-m-carborane

C

iodomesitylene
4028-63-1

iodomesitylene

D

1,3,5-trimethyl-benzene
108-67-8

1,3,5-trimethyl-benzene

Conditions
ConditionsYield
In chloroform; water mixt. of aryl(m-carboran-9-yl)iodonium tetrafluoroborate, NaF, water and chloroform was vigorously stirred under reflux at 56°C, 2.5 h; internal standard (chlorobenzene) added and org. layer was analysed by GLC;A 0%
B 100%
C 100%
D 0%
3-cyclopentadienyl-4-dimethylsulfido-8-trifluoroacetomercuro-3-ferra-1,2-dicarba-closo-dodecaborane

3-cyclopentadienyl-4-dimethylsulfido-8-trifluoroacetomercuro-3-ferra-1,2-dicarba-closo-dodecaborane

acetone
67-64-1

acetone

sodium chloride
7647-14-5

sodium chloride

8-chloromercuro-3-cyclopentadienyl-4-dimethylsulfido-3-ferra-1,2-dicarba-closo-dodecaborane acetone solvate (1:1)

8-chloromercuro-3-cyclopentadienyl-4-dimethylsulfido-3-ferra-1,2-dicarba-closo-dodecaborane acetone solvate (1:1)

Conditions
ConditionsYield
In water; acetone inert atm.; satd. aq. NaCl added slowly with stirring to a soln. of the complex in acetone at 20°C; ppt. filtered off, washed with water and dried in vacuo; recrystn. from acetone; elem. anal.;100%
C6H10(NCHC6H2C(CH3)3OHC15H10O(C(CH3)3)2)2(C6H4COOH)2

C6H10(NCHC6H2C(CH3)3OHC15H10O(C(CH3)3)2)2(C6H4COOH)2

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

sodium chloride
7647-14-5

sodium chloride

MnCl(C6H10(NCHC6H2C(CH3)3OC15H10O(C(CH3)3)2)2(C6H4COOH)2)

MnCl(C6H10(NCHC6H2C(CH3)3OC15H10O(C(CH3)3)2)2(C6H4COOH)2)

Conditions
ConditionsYield
In ethanol xanthene-compound was added to Mn(CH3CO2)2*4H2O in abs. ethanol, the soln. was refluxed in air for 2 h, cooled, aq. satd. NaCl was added, the mixt. was stirred for 10 min; extd. with CH2Cl2, the organic layer was washed with water, dried over MgSO4, the solid was rotary evapd.; elem. anal.;100%
{[(cyclopentadienyl)Co(diphenylphosphite(-1H))3]2Yb}+{CoCl3(THF)}-·2(benzene)

{[(cyclopentadienyl)Co(diphenylphosphite(-1H))3]2Yb}+{CoCl3(THF)}-·2(benzene)

sodium chloride
7647-14-5

sodium chloride

{[(cyclopentadienyl)Co(diphenylphosphite(-1H))3]2Yb}+Cl-

{[(cyclopentadienyl)Co(diphenylphosphite(-1H))3]2Yb}+Cl-

Conditions
ConditionsYield
In acetone Inert atmosphere;100%
C56H70Co2N4O4

C56H70Co2N4O4

sodium chloride
7647-14-5

sodium chloride

C56H70Cl2Co2N4O4

C56H70Cl2Co2N4O4

Conditions
ConditionsYield
Stage #1: C56H70Co2N4O4 With oxygen; toluene-4-sulfonic acid In dichloromethane for 24h;
Stage #2: sodium chloride In water
100%
ammonium hexachloridoplatinate(IV)

ammonium hexachloridoplatinate(IV)

fluorine
7782-41-4

fluorine

sodium chloride
7647-14-5

sodium chloride

sodium hexafluoridoplatinate(IV)

sodium hexafluoridoplatinate(IV)

Conditions
ConditionsYield
at 450℃; for 144h; Inert atmosphere; Milling;100%
15-crown-5
33100-27-5

15-crown-5

sodium chloride
7647-14-5

sodium chloride

zinc(II) chloride
7646-85-7

zinc(II) chloride

C10H20NaO5(1+)*Cl3Zn(1-)

C10H20NaO5(1+)*Cl3Zn(1-)

Conditions
ConditionsYield
Stage #1: 15-crown-5; sodium chloride In water at 20℃; for 12h;
Stage #2: zinc(II) chloride In ethanol for 12h; Reflux;
100%
15-crown-5
33100-27-5

15-crown-5

iron(III) chloride hexahydrate

iron(III) chloride hexahydrate

sodium chloride
7647-14-5

sodium chloride

Cl4Fe(1-)*C10H20NaO5(1+)

Cl4Fe(1-)*C10H20NaO5(1+)

Conditions
ConditionsYield
Stage #1: 15-crown-5; sodium chloride In water at 20℃; for 12h;
Stage #2: iron(III) chloride hexahydrate In ethanol for 12h; Reflux;
100%
C38H29F2NPPt(1+)*BF4(1-)

C38H29F2NPPt(1+)*BF4(1-)

sodium chloride
7647-14-5

sodium chloride

C38H29ClF2NPPt

C38H29ClF2NPPt

Conditions
ConditionsYield
In acetone at 20℃;100%
{5,10,15,20-tetrakis[4-(1-carba-closo-dodecaboran-1-yl)tetraphenyl]-17,18-dihydroporphyrin}tetracesium

{5,10,15,20-tetrakis[4-(1-carba-closo-dodecaboran-1-yl)tetraphenyl]-17,18-dihydroporphyrin}tetracesium

sodium chloride
7647-14-5

sodium chloride

{5,10,15,20-tetrakis[4-(1-carba-closo-dodecaboran-1-yl)tetraphenyl]-17,18-dihydroporphyrin}tetrasodium

{5,10,15,20-tetrakis[4-(1-carba-closo-dodecaboran-1-yl)tetraphenyl]-17,18-dihydroporphyrin}tetrasodium

Conditions
ConditionsYield
With DOWEX 50 WX8 100-200 ion exchange resin In acetone99.5%
{5,10,15,20-tetrakis[4-(1-carba-closo-dodecaboran-1-yl)tetrafluorophenyl]-17,18-dihydroporphyrin}tetracesium

{5,10,15,20-tetrakis[4-(1-carba-closo-dodecaboran-1-yl)tetrafluorophenyl]-17,18-dihydroporphyrin}tetracesium

sodium chloride
7647-14-5

sodium chloride

{5,10,15,20-tetrakis[4-(1-carba-closo-dodecaboran-1-yl)tetrafluorophenyl]-17,18-dihydroporphyrin}tetrasodium

{5,10,15,20-tetrakis[4-(1-carba-closo-dodecaboran-1-yl)tetrafluorophenyl]-17,18-dihydroporphyrin}tetrasodium

Conditions
ConditionsYield
With DOWEX 50 WX8 100-200 ion exchange resin In acetone99.5%
2-Picolinic acid
98-98-6

2-Picolinic acid

sodium chloride
7647-14-5

sodium chloride

palladium dichloride

palladium dichloride

[Pd(picolinic acid)2]
22602-40-0

[Pd(picolinic acid)2]

Conditions
ConditionsYield
In water to aq. soln. Na2(PdCl4), prepared in situ by react. PdCl2 and NaCl, was added pyridine-2-carboxylic acid in water and stirred for 2 h; ppt. was filtered, washed with water and acetone, and dried in vacuo; elem. anal.;99%
bis(diphenylphosphino)methane monooxide
23176-18-3

bis(diphenylphosphino)methane monooxide

sodium chloride
7647-14-5

sodium chloride

palladium dichloride

palladium dichloride

PdCl2((C6H5)2PCH2P(O)(C6H5)2)2
113377-86-9, 150337-07-8

PdCl2((C6H5)2PCH2P(O)(C6H5)2)2

Conditions
ConditionsYield
In methanol; dichloromethane evapn., extg. (CH2Cl2), filtering, pptn. on concg. and ether addn. (-15°C, overnight), washing (ether), drying (vac.);99%

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