2-[(4-ALLYL-2-METHOXYPHENOXY)METHYL]OXIRANE

Base Information

• Chemical Name: 2-[(4-ALLYL-2-METHOXYPHENOXY)METHYL]OXIRANE
• CAS No.: 36014-34-3
• Molecular Formula: C13H16O3
• Molecular Weight: 220.268
• Mol file: 36014-34-3.mol

Synonyms:2-[(4-ALLYL-2-METHOXYPHENOXY)METHYL]OXIRANE;1-(2-Methoxy-4-allyl-phenoxy)-2,3-epoxy-propan;4-allyl-1-(2,3-epoxy-propoxy)-2-methoxy-benzene;4-Allyl-1-(2,3-epoxy-propoxy)-2-methoxy-benzol;4-allyl-2-methoxyphenyl glycidyl ether;

Chemical Property of 2-[(4-ALLYL-2-METHOXYPHENOXY)METHYL]OXIRANE

Chemical Property:

• Boiling Point: 110 °C(Press: 0.05 Torr)
• PSA: 30.99000
• Density: 1.089±0.06 g/cm3(Predicted)
• LogP: 2.20130

Purity/Quality:

99% ^*data from raw suppliers

2-[(4-ALLYL-2-METHOXYPHENOXY)METHYL]OXIRANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-[(4-ALLYL-2-METHOXYPHENOXY)METHYL]OXIRANE

There total 3 articles about 2-[(4-ALLYL-2-METHOXYPHENOXY)METHYL]OXIRANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

4-allylguaiacol (97-53-0) + epichlorohydrin (106-89-8,24969-06-0,13403-37-7) → 3-(4-allyl-2-methoxyphenoxy)propylene 1,2-oxide (36014-34-3)

Guidance literature:

With sodium hydroxide; In water; at 85 ℃; for 0.5h;

DOI:10.1016/j.bioorg.2019.102931

Reference yield:

4-allylguaiacol (97-53-0) + epichlorohydrin (106-89-8,24969-06-0,13403-37-7) → 3-(4-allyl-2-methoxyphenoxy)propylene 1,2-oxide (36014-34-3) + C13H17ClO3

Guidance literature:

With tetra-(n-butyl)ammonium iodide; potassium carbonate; In acetonitrile; for 10h; Reflux;

DOI:10.1007/s11030-018-9867-7

Reference yield:

→ 3-(4-allyl-2-methoxyphenoxy)propylene 1,2-oxide (36014-34-3)

Guidance literature:

/BRN= 366759/, Epichlorhydrin, methanol. CH3ONa;

upstream raw materials:

4-allylguaiacol

epichlorohydrin