1-[(E)-9-(1,3-Benzodioxol-5-yl)-1-oxo-8-nonenyl]piperidine

Base Information

Chemical Name:1-[(E)-9-(1,3-Benzodioxol-5-yl)-1-oxo-8-nonenyl]piperidine
CAS No.:30505-89-6
Molecular Formula:C₂₁H₂₉NO₃
Molecular Weight:343.466
Hs Code.:
Mol file:30505-89-6.mol

Synonyms:Piperidine,1-[(8E)-9-(1,3-benzodioxol-5-yl)-1-oxo-8-nonenyl]- (9CI); Piperidine,1-[9-(1,3-benzodioxol-5-yl)-1-oxo-8-nonenyl]-, (E)-; Piperidine,1-[9-[3,4-(methylenedioxy)phenyl]-8-nonenoyl]-, (E)- (8CI); Piperolein B;Piperoleine B

Suppliers and Price of 1-[(E)-9-(1,3-Benzodioxol-5-yl)-1-oxo-8-nonenyl]piperidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-[(E)-9-(1,3-Benzodioxol-5-yl)-1-oxo-8-nonenyl]piperidine

Chemical Property:

PSA：38.77000
LogP:4.71950

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Description Also present in Piper nigrurn, this alkaloid forms a colourless oil. The piperidinyl side chain contains two more methylene groups than that in the preceding base. As before, the structure has been established by the synthesis of the alkaloid.

Technology Process of 1-[(E)-9-(1,3-Benzodioxol-5-yl)-1-oxo-8-nonenyl]piperidine

There total 3 articles about 1-[(E)-9-(1,3-Benzodioxol-5-yl)-1-oxo-8-nonenyl]piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7315-32-4
5-vinyl-1,3-benzodioxole

: 1-(piperidin-1-yl)non-8-en-1-one

: 30505-89-6
Piperolein B

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In cis-1,2-Dichloroethylene; for 48h; Reflux;
DOI:10.1039/c3ra42060d

Reference yield:

: 110-89-4
piperidine

: 31642-67-8
non-8-enoic acid

: 30505-89-6
Piperolein B

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine / N,N-dimethyl-formamide; dichloromethane / 0.5 h / 0 °C

1.2: 20 °C

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / cis-1,2-Dichloroethylene / 48 h / Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine; In cis-1,2-Dichloroethylene; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ra42060d