N-[(4-nitrophenyl)methylidene]benzenesulfonamide

Base Information

• Chemical Name: N-[(4-nitrophenyl)methylidene]benzenesulfonamide
• CAS No.: 36176-89-3
• Molecular Formula: C13H10N2O4S
• Molecular Weight: 290.299
• Hs Code.: 2935009090
• DSSTox Substance ID: DTXSID50393075
• Nikkaji Number: J323.763J
• Mol file: 36176-89-3.mol

Synonyms:N-[(4-nitrophenyl)methylidene]benzenesulfonamide;36176-89-3;DTXSID50393075;N-(4-Nitrobenzylidene)benzenesulfonamide

Chemical Property of N-[(4-nitrophenyl)methylidene]benzenesulfonamide

Chemical Property:

• PSA: 100.70000
• LogP: 4.00660
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 290.03612798
• Heavy Atom Count: 20
• Complexity: 450

Purity/Quality:

N-(4-NITRO-BENZYLIDENE)-BENZENESULFONAMIDE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)S(=O)(=O)N=CC2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of N-[(4-nitrophenyl)methylidene]benzenesulfonamide

There total 8 articles about N-[(4-nitrophenyl)methylidene]benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N,N'-di(phenylsulfonyl)selenium diimide (61945-92-4) + 4-nitrobenzaldehdye (555-16-8) → N-(p-nitrobenzylidene)benzenesulfonamide (36176-89-3)

Guidance literature:

In dichloromethane; at 30 - 40 ℃; for 2h;

Reference yield: 95.0%

benzenesulfonamide (98-10-2) + 4-nitrobenzaldehdye (555-16-8) → N-(p-nitrobenzylidene)benzenesulfonamide (36176-89-3)

Guidance literature:

With 3-methyl-1-sulphonic acid imidazolium chloride; at 20 ℃; for 0.166667h; Ionic liquid;

DOI:10.1007/BF03246053

Reference yield: 80.0%

selenoanisole (4346-64-9) + 3-(4-nitrophenyl)-2-(phenylsulfonyl)-1,2-oxaziridine (86428-23-1,78377-89-6) → phenylmethyl selenoxide (25862-09-3) + N-(p-nitrobenzylidene)benzenesulfonamide (36176-89-3)

Guidance literature:

In chloroform; for 0.0833333h;

DOI:10.1016/S0040-4020(01)96713-4

upstream raw materials:

selenoanisole

3-(4-nitrophenyl)-2-(phenylsulfonyl)-1,2-oxaziridine

benzenesulfonamide

4-nitrobenzaldehdye

Downstream raw materials:

4-nitrophenyl(phenyl)methanol

4-methylphenyl(4-nitrophenyl)methanol

2-p-nitrophenyl-N-phenylsulphonylaziridine

3-(4-nitrophenyl)-2-(phenylsulfonyl)-1,2-oxaziridine