Glycine, N-[(4-methylphenyl)sulfonyl]-, hydrazide

Base Information

Chemical Name:Glycine, N-[(4-methylphenyl)sulfonyl]-, hydrazide
CAS No.:3619-20-3
Molecular Formula:C9H13N3O3S
Molecular Weight:243.287
Hs Code.:
Mol file:3619-20-3.mol

Synonyms:N-(toluene-4-sulfonyl)-glycine hydrazide;p-Tosylglycin-hydrazid;N-(4-toluenesulfonyl)-glycinyl hydrazide;N-Hydrazinocarbonylmethyl-4-methyl-benzenesulfonamide;N-(Toluol-4-sulfonyl)-glycin-hydrazid;N--glycinhydrazid;Tosyl-glycinhydrazid;

Suppliers and Price of Glycine, N-[(4-methylphenyl)sulfonyl]-, hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
N-(2-Hydrazinyl-2-oxoethyl)-4-methylbenzenesulfonamide 97%
5g
$ 874.00

Total 1 raw suppliers

Chemical Property of Glycine, N-[(4-methylphenyl)sulfonyl]-, hydrazide

Chemical Property:

Melting Point:155 - 156 °C
PSA：109.67000
LogP:1.82610

Purity/Quality:

95% ^*data from raw suppliers

N-(2-Hydrazinyl-2-oxoethyl)-4-methylbenzenesulfonamide 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Glycine, N-[(4-methylphenyl)sulfonyl]-, hydrazide

There total 5 articles about Glycine, N-[(4-methylphenyl)sulfonyl]-, hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.4%

: 2645-02-5
methyl tosylglycinate

: 3619-20-3
p-methylphenylsulfonylaminoacetic acid hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 6h; Reflux;
DOI:10.1111/j.1747-0285.2010.01050.x

Reference yield:

: N-(toluene-4-sulfonyl)-glycine-(N'-benzyloxycarbonyl-hydrazide)

: 3619-20-3
p-methylphenylsulfonylaminoacetic acid hydrazide

Guidance literature:: With hydrogenchloride; palladium; Hydrogenation;
DOI:10.1021/ja01122a057

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 3619-20-3
p-methylphenylsulfonylaminoacetic acid hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 20 h / 20 °C / Cooling with ice

2: hydrazine hydrate / ethanol / 6 h / Reflux

With dmap; hydrazine hydrate; triethylamine; In ethanol; dichloromethane;
DOI:10.1111/j.1747-0285.2010.01050.x