3-[(DIMETHYLAMINO)METHYL]-4-[4-(METHYLSULFANYL)PHENOXY]BENZENE-1-SULFONAMIDE

Base Information

• Chemical Name: 3-[(DIMETHYLAMINO)METHYL]-4-[4-(METHYLSULFANYL)PHENOXY]BENZENE-1-SULFONAMIDE
• CAS No.: 364321-71-1
• Molecular Formula: C16H20N2O3S2
• Molecular Weight: 352.478
• Mol file: 364321-71-1.mol

Synonyms:UNII-W26I0D1D6J;3-[(DIMETHYLAMINO)METHYL]-4-[4-(METHYLSULFANYL)PHENOXY]BENZENE-1-SULFONAMIDE;3-[(dimethylamino)methyl]-4-[4-(methylsulfanyl)phenoxy]benzenesulfonamide;3-((dimethylamino)methyl)-4-(4-(methylthio)phenoxy)benzenesulfonamide;Uk-390,957;

Chemical Property of 3-[(DIMETHYLAMINO)METHYL]-4-[4-(METHYLSULFANYL)PHENOXY]BENZENE-1-SULFONAMIDE

Chemical Property:

• PSA: 106.31000
• LogP: 4.69090

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-[(DIMETHYLAMINO)METHYL]-4-[4-(METHYLSULFANYL)PHENOXY]BENZENE-1-SULFONAMIDE

There total 2 articles about 3-[(DIMETHYLAMINO)METHYL]-4-[4-(METHYLSULFANYL)PHENOXY]BENZENE-1-SULFONAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

3-[(dimethylamino)methyl]-4-[4-(methylthio)phenoxy]benzenesulfonic acid (849064-08-0) → UK-390957 (364321-71-1)

Guidance literature:

3-[(dimethylamino)methyl]-4-[4-(methylthio)phenoxy]benzenesulfonic acid; With trichlorophosphate; In acetonitrile; at 81 ℃; for 2h;

With ammonia; In water; acetonitrile; at -10 - 40 ℃; Heating / reflux;

Reference yield:

→ UK-390957 (364321-71-1) + N,N-Dimethyl-N-{5-nitro-2-[4-(trifluoromethyl)phenoxy]benzyl}amine

Guidance literature:

Reference yield: 86.0%

UK-390957 (364321-71-1) + acetyl chloride (75-36-5) → N-Acetyl-3-[(dimethylamino)methyl]-4-[4-(methylsulfanyl)phenoxy]-benzenesulfonamide

Guidance literature:

With triethylamine; In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran;

upstream raw materials:

3-[(dimethylamino)methyl]-4-[4-(methylthio)phenoxy]benzenesulfonic acid

Downstream raw materials:

3-[(dimethylamino)methyl]-4-[4-(methylthio)phenoxy]benzenesulfonamide (R,R)-tartrate

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