tert-butyl 3-Mercaptopyridin-4-ylcarbaMate

Base Information

• Chemical Name: tert-butyl 3-Mercaptopyridin-4-ylcarbaMate
• CAS No.: 365996-04-9
• Molecular Formula: C10H14N2O2S
• Molecular Weight: 226.29500
• Hs Code.: 2933399090
• Mol file: 365996-04-9.mol

Synonyms:tert-Butyl 3-sulfanylpyridin-4-ylcarbamate;3-sulfanylpyridin-4-ylcarbamic acid tert-butyl ester;

Chemical Property of tert-butyl 3-Mercaptopyridin-4-ylcarbaMate

Chemical Property:

• PSA: 93.25000
• LogP: 2.13920
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl(3-mercaptopyridin-4-yl)carbamate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-butyl 3-Mercaptopyridin-4-ylcarbaMate

There total 2 articles about tert-butyl 3-Mercaptopyridin-4-ylcarbaMate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

N-(4-pyridyl) t-butyl carbamate (98400-69-2) → 4-[(tert-Butoxycarbonyl)amino]-3-mercaptopyridine (365996-04-9)

Guidance literature:

N-(4-pyridyl) t-butyl carbamate; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 2h;

With sulfur; In tetrahydrofuran; hexane; at -78 - 20 ℃;

DOI:10.3987/COM-04-10071

Reference yield:

hydrogen sulfide (7783-06-4) + N-(4-pyridyl) t-butyl carbamate (98400-69-2) → 4-[(tert-Butoxycarbonyl)amino]-3-mercaptopyridine (365996-04-9)

Guidance literature:

With hydrogenchloride; n-butyllithium; In tetrahydrofuran; hexane; dichloromethane; water;

Reference yield: 45.0%

4-[(tert-Butoxycarbonyl)amino]-3-mercaptopyridine (365996-04-9) → thiazolo[5,4-c]-pyridine (273-70-1)

Guidance literature:

In formic acid; for 2h; Heating;

DOI:10.3987/COM-04-10071

upstream raw materials:

N-(4-pyridyl) t-butyl carbamate

hydrogen sulfide

Downstream raw materials:

thiazolo[5,4-c]-pyridine

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