3-methoxy-N-(4-methoxyphenyl)aniline

Base Information

• Chemical Name: 3-methoxy-N-(4-methoxyphenyl)aniline
• CAS No.: 3661-49-2
• Molecular Formula: C14H15NO2
• Molecular Weight: 229.279
• DSSTox Substance ID: DTXSID60577223
• Nikkaji Number: J2.135.912B
• Wikidata: Q82467173

Synonyms:3-methoxy-N-(4-methoxyphenyl)aniline;3661-49-2;3,4'-Dimethoxydiphenylamine;SCHEMBL2112594;DTXSID60577223;WETFGWQHUYDJDK-UHFFFAOYSA-N;MFCD22084029;SB76848;3-Methoxy-N-(4-methoxyphenyl)benzenamine;BS-44203;M3065;T72369

Chemical Property of 3-methoxy-N-(4-methoxyphenyl)aniline

Chemical Property:

• XLogP3: 3.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 229.110278721
• Heavy Atom Count: 17
• Complexity: 214

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)NC2=CC(=CC=C2)OC

Technology Process of 3-methoxy-N-(4-methoxyphenyl)aniline

There total 18 articles about 3-methoxy-N-(4-methoxyphenyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

para-iodoanisole (696-62-8) + m-Anisidine (536-90-3,918666-97-4) → 3-methoxy-N-(4-methoxyphenyl)benzenamine (3661-49-2)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 100 ℃; for 20h; Inert atmosphere;

DOI:10.1002/asia.201501239

Reference yield: 99.0%

1-chloro-3-methoxy-benzene (2845-89-8) + 4-methoxy-aniline (104-94-9) → 3-methoxy-N-(4-methoxyphenyl)benzenamine (3661-49-2)

Guidance literature:

With sodium t-butanolate; palladium diacetate; (R)-(-)-1-[(S)-2-(dicyclohexylphosphino)ferrocenyl]ethyl di-t-butylphosphine; In 1,2-dimethoxyethane; at 100 ℃; for 24h;

DOI:10.1021/ja077074w

Reference yield: 97.0%

3-methoxyphenyl bromide (2398-37-0) + 4-methoxy-aniline (104-94-9) → 3-methoxy-N-(4-methoxyphenyl)benzenamine (3661-49-2)

Guidance literature:

With copper(l) iodide; potassium carbonate; L-proline; In dimethyl sulfoxide; at 90 ℃; for 40h;

DOI:10.1021/jo0504464

upstream raw materials:

3-(4-methoxy phenylamino)phenol

dimethyl sulfate

m-Methoxyphenyllead(IV) triacetate

4-methoxy-aniline

Downstream raw materials:

2-methoxy-N⁴-(4-methoxy-phenyl)-p-phenylenediamine

[(3-methoxyphenyl)-4-methoxyphenylamino]acetonitrile

N²,N²,N^2',N^2',N⁷,N⁷,N^7',N^7'-octakis(3-methoxypheny)-9,9'-spirobi[fluorene]-2,2',7,7'-tetraamine

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