2-Methoxy-6-[2-(4-methoxyphenyl)ethyl]benzoic acid

Base Information

• Chemical Name: 2-Methoxy-6-[2-(4-methoxyphenyl)ethyl]benzoic acid
• CAS No.: 36640-14-9
• Molecular Formula: C17H18O4
• Molecular Weight: 286.328
• Hs Code.: 2918990090
• Mol file: 36640-14-9.mol

Synonyms:2-METHOXY-6-[2-(4-METHOXY-PHENYL)-ETHYL]-BENZOIC ACID;2-METHOXY-6-[2-(4-METHOXYPHENYL)ETHYL]BENZOIC ACID;

Chemical Property of 2-Methoxy-6-[2-(4-methoxyphenyl)ethyl]benzoic acid

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• PSA: 55.76000
• LogP: 3.18720

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Methoxy-6-[2-(4-methoxyphenyl)ethyl]benzoic acid

There total 25 articles about 2-Methoxy-6-[2-(4-methoxyphenyl)ethyl]benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3,4'-dimethylstilbene-2-carboxylic acid (113345-85-0) → 2-Methoxy-6-<2-(4-methoxyphenyl)ethyl>benzoic acid (36640-14-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 5h; under 2844.3 - 3102.9 Torr;

Reference yield: 90.0%

3,4'-Dimethoxybibenzyl-2-carbonsaeureethylester (118842-86-7) → 2-Methoxy-6-<2-(4-methoxyphenyl)ethyl>benzoic acid (36640-14-9)

Guidance literature:

With potassium hydroxide; In methanol; for 12h; Heating;

DOI:10.1055/s-1988-27624

Reference yield: 85.0%

Di-O-methyllunarsaeuremethylester (63898-02-2) → 2-Methoxy-6-<2-(4-methoxyphenyl)ethyl>benzoic acid (36640-14-9)

Guidance literature:

With potassium hydroxide; In ethanol; water; for 96h; Heating;

upstream raw materials:

3,4'-dimethylstilbene-2-carboxylic acid

N-Methyl-N-nitroso-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

3,4'-Dimethoxybibenzyl-2-carbonsaeureethylester

Di-O-methyllunarsaeuremethylester

Downstream raw materials:

Lunularsaeureamid

3,4'-Dimethoxybibenzyl-2-carbonsaeureamid

Lunularsaeurediethylamid

N,N-Diethyl-2-methoxy-6-[2-(4-methoxy-phenyl)-ethyl]-benzamide

Refernces

• 1、 Nakayama, Takato,Fukushi, Yukiharu,Mizutani, Junya,Tahara, Satoshi. "Inhibiting effects of lunularic acid analogs on the growth of liverwort, watercress, and timothy grass". . p. 862 - 865. Retrieved 2007/10/03.
• 2、 Mali, Raghao S.,Shelke, Dattatray W.. "Convenient syntheses of 3-aryl-3,4-dihydroisocoumarins and lunularic acid derivatives". . p. 822 - 825. Retrieved 2007/10/02.