2-iodo-N-(3-methoxyphenyl)benzamide

Base Information

Chemical Name:2-iodo-N-(3-methoxyphenyl)benzamide
CAS No.:36684-48-7
Molecular Formula:C14H12INO2
Molecular Weight:353.159
Hs Code.:
DSSTox Substance ID:DTXSID00359964
Wikidata:Q82141422
Mol file:36684-48-7.mol

Synonyms:2-iodo-N-(3-methoxyphenyl)benzamide;36684-48-7;Benzamide, 2-iodo-N-(3-methoxyphenyl)-;Cambridge id 5335433;Oprea1_573203;DTXSID00359964;STK201929;AKOS001604818;EU-0069645;AB00081213-01;AG-690/09446014;SR-01000414654;A1-05016;SR-01000414654-1

Suppliers and Price of 2-iodo-N-(3-methoxyphenyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
2-Iodo-N-(3-methoxyphenyl)benzamide 95%
5g
$ 1320.00

American Custom Chemicals Corporation
2-IODO-N-(3-METHOXYPHENYL)BENZAMIDE 95.00%
5MG
$ 501.39

A1 Biochem Labs
2-Iodo-N-(3-methoxyphenyl)benzamide 95%
5 g
$ 800.00

Total 0 raw suppliers

Chemical Property of 2-iodo-N-(3-methoxyphenyl)benzamide

Chemical Property:

PSA：41.82000
LogP:3.93610
XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:352.99128
Heavy Atom Count:18
Complexity:285

Purity/Quality:: 2-Iodo-N-(3-methoxyphenyl)benzamide 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1)NC(=O)C2=CC=CC=C2I

Technology Process of 2-iodo-N-(3-methoxyphenyl)benzamide

There total 4 articles about 2-iodo-N-(3-methoxyphenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 88-67-5
2-Iodobenzoic acid

: 536-90-3,918666-97-4
m-Anisidine

: 36684-48-7
2-iodo-N-(3-methoxy-phenyl)-benzamide

Guidance literature:: 2-Iodobenzoic acid; With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; at 20 ℃; for 0.166667h;

m-Anisidine; at 20 ℃; for 1h;
DOI:10.1039/c8ob00653a

Reference yield:

: 609-67-6
2-Iodobenzoyl chloride

: 536-90-3,918666-97-4
m-Anisidine

: 36684-48-7
2-iodo-N-(3-methoxy-phenyl)-benzamide

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/adsc.201301020

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 36684-48-7
2-iodo-N-(3-methoxy-phenyl)-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / N,N-dimethyl-formamide / 3 h / 80 °C

2: pyridine / dichloromethane / 0 - 20 °C

With pyridine; thionyl chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201301020